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天然矿物材料在有机硅压敏胶中的应用研究

Study of Applying Naturally Occurring Mineral Materials for Silicone Pressure-Sensitive Adhesives.

作者信息

Antosik Adrian Krzysztof, Kucharska Edyta, Mozelewska Karolina

机构信息

Department of Chemical Organic Technology and Polymeric Materials, Faculty of Chemical Technology and Engineering, West Pomeranian University of Technology, 70-322 Szczecin, Poland.

出版信息

Materials (Basel). 2023 Mar 3;16(5):2092. doi: 10.3390/ma16052092.

DOI:10.3390/ma16052092
PMID:36903207
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10004305/
Abstract

Silicones are commonly used as adhesives when high-quality materials are required due to harsh environmental conditions such as high temperature, humidity, etc. To ensure high resistance to environmental conditions, including high temperatures, modifications of silicone adhesives are made using fillers. The characteristics of a modified silicone-based pressure-sensitive adhesive with filler are the focus of this work. Functionalized palygorskite was prepared in this investigation by grafting 3-mercaptopropyltrimethoxysilane (MPTMS) onto palygorskite (palygorskite-MPTMS). The palygorskite was functionalized using MPTMS under dried conditions. FTIR/ATR spectroscopy, thermogravimetric analysis, and elemental analysis were all used to characterize the obtained palygorskite-MPTMS. MPTMS loading onto palygorskite was also proposed. The results demonstrated that palygorskite's initial calcination favors the grafting of functional groups on its surface. New self-adhesive tapes based on palygorskite-modified silicone resins have been obtained. This functionalized filler allows for the improvement of the compatibility of palygorskite with specific resins for application in heat-resistant silicone pressure-sensitive adhesives. The new self-adhesive materials showed increased thermal resistance while maintaining good self-adhesive properties.

摘要

由于高温、高湿等恶劣环境条件需要高质量材料时，硅氧烷通常用作粘合剂。为确保对包括高温在内的环境条件具有高耐受性，使用填料对硅氧烷粘合剂进行改性。本研究重点关注含填料的改性硅基压敏粘合剂的特性。在本研究中，通过将3-巯丙基三甲氧基硅烷（MPTMS）接枝到坡缕石（坡缕石-MPTMS）上制备了功能化坡缕石。在干燥条件下使用MPTMS对坡缕石进行功能化。FTIR/ATR光谱、热重分析和元素分析均用于表征所得的坡缕石-MPTMS。还提出了MPTMS在坡缕石上的负载量。结果表明，坡缕石的初始煅烧有利于其表面官能团的接枝。已获得基于坡缕石改性硅树脂的新型自粘胶带。这种功能化填料可提高坡缕石与特定树脂的相容性，用于耐热硅基压敏粘合剂。新型自粘材料在保持良好自粘性能的同时，耐热性增强。

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