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黏附条件对用于最终修复体的3D打印树脂热循环后剪切黏结强度的影响

Effect of Adhesion Conditions on the Shear Bond Strength of 3D Printing Resins after Thermocycling Used for Definitive Prosthesis.

作者信息

Kang You-Jung, Park Yeseul, Shin Yooseok, Kim Jee-Hwan

机构信息

Department of Prosthodontics, Oral Science Research Center, College of Dentistry, Yonsei University, Seoul 03722, Republic of Korea.

Department of Conservative Dentistry, Oral Science Research Center, College of Dentistry, Yonsei University, Seoul 03722, Republic of Korea.

出版信息

Polymers (Basel). 2023 Mar 10;15(6):1390. doi: 10.3390/polym15061390.

Abstract

Three-dimensional (3D) printing polymers such as urethane dimethacrylate (UDMA) and ethoxylated bisphenol A dimethacrylate (Bis-EMA) are typically used in definitive prosthesis and require surface treatments before bonding. However, surface treatment and adhesion conditions often affect long-term use. Herein, polymers were divided into Groups 1 and 2 for the UDMA and Bis-EMA components, respectively. The shear bond strength (SBS) between two types of 3D printing resins and resin cements was measured using Rely X Ultimate Cement and Rely X U200, according to adhesion conditions such as single bond universal (SBU) and airborne-particle abrasion (APA) treatments. Thermocycling was performed to evaluate the long-term stability. Sample surface changes were observed using a scanning electron microscope and surface roughness measuring instrument. The effect of interaction between the resin material and adhesion conditions on the SBS was analyzed via a two-way analysis of variance. The optimal adhesion condition for Group 1 was achieved when U200 was used after APA and SBU, whereas Group 2 was not significantly affected by the adhesion conditions. After thermocycling, the SBS significantly decreased in Group 1 without APA treatment and in the entire Group 2. Additionally, porosity, along with increased roughness, was observed on both material surfaces after APA.

摘要

三维(3D)打印聚合物,如聚氨酯二甲基丙烯酸酯(UDMA)和乙氧基化双酚A二甲基丙烯酸酯(Bis-EMA),通常用于定制假体,在粘结前需要进行表面处理。然而,表面处理和粘结条件往往会影响其长期使用。在此,聚合物分别针对UDMA和Bis-EMA成分分为第1组和第2组。根据单键通用(SBU)和空气颗粒磨损(APA)处理等粘结条件,使用Rely X Ultimate Cement和Rely X U200测量两种3D打印树脂与树脂水门汀之间的剪切粘结强度(SBS)。进行热循环以评估长期稳定性。使用扫描电子显微镜和表面粗糙度测量仪观察样品表面变化。通过双向方差分析分析树脂材料与粘结条件之间的相互作用对SBS的影响。第1组在APA和SBU处理后使用U200时达到最佳粘结条件,而第2组不受粘结条件的显著影响。热循环后,未进行APA处理的第1组和整个第2组的SBS显著降低。此外,APA处理后,两种材料表面均观察到孔隙率增加以及粗糙度增加。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/d58e/10056338/116a1e357e4a/polymers-15-01390-g001.jpg

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