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直接树脂复合材料与CAD-CAM复合树脂块的剪切粘结强度:微机械和化学块体表面处理的相对贡献

Shear Bond Strength of a Direct Resin Composite to CAD-CAM Composite Blocks: Relative Contribution of Micromechanical and Chemical Block Surface Treatment.

作者信息

Fouquet Vincent, Lachard François, Abdel-Gawad Sarah, Dursun Elisabeth, Attal Jean-Pierre, François Philippe

机构信息

Innovative Dental Materials and Interfaces Research Unit (URB2i, UR4462), Faculty of Health, Paris Cité University, 1 Rue Maurice Arnoux, 92120 Montrouge, France.

Department of Prosthetic Dentistry, Louis Mourier Hospital, 178 Rue des Renouillers, 92700 Colombes, France.

出版信息

Materials (Basel). 2022 Jul 19;15(14):5018. doi: 10.3390/ma15145018.

Abstract

This study aims to compare the shear bond strength (SBS) of a direct resin composite to CAD-CAM resin composite blocks treated with different surface treatments: micromechanical, chemical or a combination of both. Eight CAD-CAM resin composite blocks, namely Brilliant Crios, Cerasmart 270, Vita Enamic, Grandio block, Katana Avencia, Lava Ultimate, Tetric CAD and Shofu Block HC were chosen. The micromechanical surface treatment protocols tested were hydrofluoric acid, polyacrylic acid or sandblasting, and the chemical one was a universal primer. These treated CAD-CAM blocks were tested to determine the SBS of a light-curing composite resin Z100 bonded to their surface. Two-way ANOVA followed by Tukey's post hoc test was used to investigate the difference in SBS. Failures were analyzed by Fisher's exact test. Bonding interfaces were examined by scanning electron microscopy. The micromechanical surface treatments give the highest SBS values: sandblasting appears to be the most efficient procedure for dispersed filler composite blocks, while hydrofluoric acid etching is preferable for polymer-infiltrated ceramic network (PICN) blocks. The use of universal primer does not improve SBS values on dispersed filler composite blocks. For PICN blocks, the use of universal primer significantly increases SBS values when combined with hydrofluoric acid etching.

摘要

本研究旨在比较直接树脂复合材料与经不同表面处理(微机械处理、化学处理或两者结合)的CAD-CAM树脂复合材料块的剪切粘结强度(SBS)。选择了八个CAD-CAM树脂复合材料块,即Brilliant Crios、Cerasmart 270、Vita Enamic、Grandio block、Katana Avencia、Lava Ultimate、Tetric CAD和Shofu Block HC。测试的微机械表面处理方案有氢氟酸、聚丙烯酸或喷砂处理,化学处理方案是使用通用底漆。对这些经过处理的CAD-CAM块进行测试,以确定粘结在其表面的光固化复合树脂Z100的SBS。采用双向方差分析并随后进行Tukey事后检验来研究SBS的差异。通过Fisher精确检验分析失败情况。通过扫描电子显微镜检查粘结界面。微机械表面处理给出了最高的SBS值:喷砂处理似乎是分散填料复合块最有效的处理方法,而氢氟酸蚀刻对于聚合物渗透陶瓷网络(PICN)块更可取。在分散填料复合块上使用通用底漆并不能提高SBS值。对于PICN块,当与氢氟酸蚀刻结合使用时,通用底漆的使用会显著提高SBS值。

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