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采用喷雾干燥法用不同壁材对牛至精油进行包封。

Encapsulation of Origanum onites essential oil with different wall material using spray drying.

作者信息

Balci-Torun Ferhan

机构信息

Faculty of Tourism, Department of Gastronomy and Culinary Art, Akdeniz University, Antalya, Turkey.

出版信息

Phytochem Anal. 2024 Dec;35(8):1736-1747. doi: 10.1002/pca.3218. Epub 2023 Mar 29.

Abstract

INTRODUCTION

Origanum onites has antibacterial, antifungal, and antioxidant properties due to its essential oil. The fact that these oils are sensitive to environmental conditions causes the need for advanced processing technologies.

OBJECTIVE

This study was aimed to encapsulate essential oil of O. onites by spray drying to extend its shelf life.

METHODS

Spray drying was used to encapsulate the essential oil of O. onites, which was then mixed with maltodextrin, arabic gum, and β-cyclodextrin using response surface methodology. After 60 days of storage, aroma analysis was performed on the essential oil of O. onites and the essential oil powder that was produced under ideal conditions.

RESULTS

O. onites essential oil powder was subjected to GC-MS analysis to identify 72 aroma components. Carvacrol and linalool concentrations varied from 22.66 to 30.11 mg/g and from 32.25 to 53.57 mg/g, respectively. The spray-dried microcapsules' D values ranged from 40.75 to 48.95 μm. For every trial, the drying yield and solubility values were higher than 60% and 90%, respectively. The results of the surface optimization showed that the ideal inlet air temperature was 190°C and the ideal concentration of β-cyclodextrin in the wall material was 1%.

CONCLUSION

The findings indicate that O. onites essential oil was successfully encapsulated via spray drying. The preservation of critical aroma compounds in the resulting capsules is high.

摘要

引言

牛至因其精油具有抗菌、抗真菌和抗氧化特性。这些精油对环境条件敏感,因此需要先进的加工技术。

目的

本研究旨在通过喷雾干燥封装牛至精油以延长其保质期。

方法

采用喷雾干燥法封装牛至精油,然后使用响应面法将其与麦芽糊精、阿拉伯胶和β-环糊精混合。储存60天后,对牛至精油和在理想条件下制备的精油粉末进行香气分析。

结果

对牛至精油粉末进行气相色谱-质谱联用(GC-MS)分析,以鉴定72种香气成分。香芹酚和芳樟醇浓度分别在22.66至30.11mg/g和32.25至53.57mg/g之间变化。喷雾干燥微胶囊的D值在40.75至48.95μm之间。每次试验的干燥产率和溶解度值分别高于60%和90%。表面优化结果表明,理想的进风温度为190°C,壁材中β-环糊精的理想浓度为1%。

结论

研究结果表明,牛至精油通过喷雾干燥成功封装。所得胶囊中关键香气化合物的保留率很高。

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