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沉积在适用于骨科的316钢和Ti6Al4V钛合金上的氧化石墨烯的激光发射光谱

Laser Emission Spectroscopy of Graphene Oxide Deposited on 316 Steel and Ti6Al4V Titanium Alloy Suitable for Orthopedics.

作者信息

Nasiłowska Barbara, Skrzeczanowski Wojciech, Bombalska Aneta, Bogdanowicz Zdzisław

机构信息

Institute of Optoelectronics, Military University of Technology, gen. S. Kaliskiego 2, 00-908 Warsaw, Poland.

Faculty of Mechanical Engineering, Military University of Technology, gen. S. Kaliskiego 2, 00-908 Warsaw, Poland.

出版信息

Materials (Basel). 2023 Mar 24;16(7):2574. doi: 10.3390/ma16072574.

DOI:10.3390/ma16072574
PMID:37048868
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10095499/
Abstract

This paper presents the results of an analysis of carbon (in the form of graphene oxide) deposited on the surface of threads made from stainless steel 316 and titanium alloy Ti6Al4V used in orthopedics using Laser Induced Breakdown Spectroscopy (LIBS). The aim of the article is to indicate the possibility of using the LIBS spectra for the study of thin layers, including graphene derivatives and other elements. Stratigraphic measurements allowed the detection of differences in the spectra peaks of individual elements, not only in the surface layer itself and in the native material, but also in the intermediate layer connecting the two layers. Due to the clear difference in the outline of the spectrum of graphene oxide and the spectrum of the native material of the samples analyzed, a clear incorporation of carbon atoms into the surface layer was observed. A factor analysis was performed, which confirmed the incorporation of graphene oxide into the surface layer of the native material of the elements examined.

摘要

本文介绍了使用激光诱导击穿光谱法（LIBS）对沉积在用于骨科的316不锈钢和钛合金Ti6Al4V制成的螺纹表面上的碳（以氧化石墨烯形式）进行分析的结果。本文的目的是指出使用LIBS光谱研究包括石墨烯衍生物和其他元素在内的薄层的可能性。地层测量不仅可以检测到各元素光谱峰在表层本身和原生材料中的差异，还可以检测到连接这两层的中间层中的差异。由于所分析样品的氧化石墨烯光谱与原生材料光谱在轮廓上存在明显差异，因此观察到碳原子明显掺入到表层中。进行了因子分析，证实了氧化石墨烯掺入到所检测元素原生材料的表层中。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/80c4/10095499/a679012796da/materials-16-02574-g011.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/80c4/10095499/12a1712d2030/materials-16-02574-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/80c4/10095499/b62f5a0cf784/materials-16-02574-g008.jpg
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https://cdn.ncbi.nlm.nih.gov/pmc/blobs/80c4/10095499/a679012796da/materials-16-02574-g011.jpg

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