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通过激光粉末床熔融制造的孔隙率渐变β-Ti21S三重周期极小曲面多孔结构的计量表征。

Metrological characterization of porosity graded β-Ti21S triply periodic minimal surface cellular structure manufactured by laser powder bed fusion.

作者信息

Emanuelli Lorena, De Biasi Raffaele, Fu Huijuan, du Plessis Anton, Lora Carlo, Jam Alireza, Benedetti Matteo, Pellizzari Massimo

机构信息

INSTM (Operative center: University of Trento), Trento, 38123, Italy.

Department of Industrial Engineering, University of Trento, Trento, Italy.

出版信息

Int J Bioprint. 2023 Apr 7;9(4):729. doi: 10.18063/ijb.729. eCollection 2023.

Abstract

The design of a functionally graded porous structure (FGPS) for use in prosthetic devices is crucial for meeting both mechanical and biological requirements. One of the most commonly used cellular structures in FGPS is the triply periodic minimal surface (TPMS) structure due to its ability to be defined by implicit equations, which allows for smooth transitions between layers. This study evaluates the feasibility of using a novel β-Ti21S alloy to fabricate TPMS-based FGPS. This beta titanium alloy exhibits low elastic modulus (53 GPa) and good mechanical properties in as-built condition. Two TPMS FGPSs with relative density gradients of 0.17, 0.34, 0.50, 0.66, and 0.83 and unit cell sizes of 2.5 mm and 4 mm were designed and fabricated using laser powder bed fusion (LPBF). The as-manufactured structures were analyzed using scanning electron microscopy (SEM) and X-ray micro-computed tomography (μ-CT), and the results were compared to the design. The analysis revealed that the pore size and ligament thickness were undersized by less than 5%. Compression tests showed that the stabilized elastic modulus was 4.1 GPa for the TPMS with a 2.5 mm unit cell size and 10.7 GPa for the TPMS with a 4 mm unit cell size. A finite element simulation was performed to predict the specimen's elastic properties, and a lumped model based on lattice homogenized properties was proposed and its limitations were explored.

摘要

用于假体装置的功能梯度多孔结构(FGPS)的设计对于满足机械和生物学要求至关重要。功能梯度多孔结构中最常用的多孔结构之一是三重周期极小曲面(TPMS)结构,因为它能够由隐式方程定义,这使得各层之间能够实现平滑过渡。本研究评估了使用新型β-Ti21S合金制造基于TPMS的功能梯度多孔结构的可行性。这种β钛合金在铸态条件下表现出低弹性模量(53 GPa)和良好的机械性能。使用激光粉末床熔融(LPBF)设计并制造了两个相对密度梯度分别为0.17、0.34、0.50、0.66和0.83且单胞尺寸分别为2.5 mm和4 mm的基于TPMS的功能梯度多孔结构。使用扫描电子显微镜(SEM)和X射线显微计算机断层扫描(μ-CT)对制造后的结构进行了分析,并将结果与设计进行了比较。分析表明,孔径和韧带厚度的尺寸不足小于5%。压缩试验表明,单胞尺寸为2.5 mm的基于TPMS的功能梯度多孔结构的稳定弹性模量为4.1 GPa,单胞尺寸为4 mm的基于TPMS的功能梯度多孔结构的稳定弹性模量为10.7 GPa。进行了有限元模拟以预测试样的弹性性能,并提出了基于晶格均匀化性能的集总模型并探讨了其局限性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/73a3/10272211/613f20675336/IJB-9-4-729-g001.jpg

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