Kojima T, Okamoto I, Miyazaki T, Chikasue F, Yashiki M, Nakamura K
Forensic Sci Int. 1986 Jun;31(2):93-102. doi: 10.1016/0379-0738(86)90193-3.
A 28-year-old male methamphetamine abuser, who had been buried for 5 years after being killed by strangulation, was found skeletonized. Methamphetamine and amphetamine in the significantly denatured fatty material of the bone marrow were analyzed by gas chromatography and gas chromatography-mass spectrometry. The confirmation of the chemicals was carried out by chemical ionization (CI) mass chromatography, CI mass spectrometry and CI mass fragmentography. The concentrations of methamphetamine and amphetamine determined by CI mass fragmentography were 1.0 mumol/100 g and 0.1 mumol/100 g, respectively. The method used would seem to be very useful for determination of methamphetamine and amphetamine in marked putrefied biological materials.
一名28岁男性甲基苯丙胺滥用者,被勒死后掩埋5年,被发现已成骨架。通过气相色谱法和气相色谱-质谱联用仪分析了骨髓中显著变性的脂肪物质中的甲基苯丙胺和苯丙胺。通过化学电离(CI)质谱色谱法、CI质谱分析法和CI质谱碎片分析法对这些化学物质进行确证。通过CI质谱碎片分析法测定的甲基苯丙胺和苯丙胺浓度分别为1.0 μmol/100 g和0.1 μmol/100 g。所采用的方法对于测定高度腐败生物材料中的甲基苯丙胺和苯丙胺似乎非常有用。