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微波、超声波及其组合在含氮双环杂环合成中的应用。

The Application of Microwaves, Ultrasounds, and Their Combination in the Synthesis of Nitrogen-Containing Bicyclic Heterocycles.

机构信息

Department of Pharmacy, "Federico II" University of Naples, 80131 Naples, Italy.

Department of Medicine, Surgery and Pharmacy, University of Sassari, 07100 Sassari, Italy.

出版信息

Int J Mol Sci. 2023 Jun 27;24(13):10722. doi: 10.3390/ijms241310722.

DOI:10.3390/ijms241310722
PMID:37445897
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC10341901/
Abstract

The use of alternative energy sources, such as microwaves (MW) or ultrasounds (US), and their mutual cross-combination have been widely described in the literature in the development of new synthetic methodologies in organic and medicinal chemistry. In this review, our attention is focused on representative examples, reported in the literature in the year range 2013-2023 of selected N-containing bicyclic heterocycles, with the aim to highlight the advantages of microwave- and ultrasound-assisted organic synthesis.

摘要

在有机和药物化学的新合成方法学的发展中，替代能源（如微波（MW）或超声波（US））的使用及其相互交叉组合在文献中已有广泛描述。在这篇综述中，我们的注意力集中在文献中报道的 2013 年至 2023 年的选定含氮双环杂环的有代表性的例子上，目的是强调微波和超声波辅助有机合成的优势。

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RSC Adv. 2020 Apr 7;10(24):14170-14197. doi: 10.1039/d0ra01378a. eCollection 2020 Apr 6.
6
Engineered N-doped graphene quantum dots/CoFeO spherical composites as a robust and retrievable catalyst: fabrication, characterization, and catalytic performance investigation in microwave-assisted synthesis of quinoline-3-carbonitrile derivatives.工程化氮掺杂石墨烯量子点/CoFeO球形复合材料作为一种坚固且可回收的催化剂：喹啉-3-甲腈衍生物微波辅助合成中的制备、表征及催化性能研究
RSC Adv. 2021 Oct 27;11(55):34724-34734. doi: 10.1039/d1ra05739a. eCollection 2021 Oct 25.
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The Highly Efficient Synthesis of 1,2-Disubstituted Benzimidazoles Using Microwave Irradiation.微波辐射促进 1,2-二取代苯并咪唑的高效合成。
Molecules. 2022 Mar 7;27(5):1751. doi: 10.3390/molecules27051751.
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Green Chemistry in the Synthesis of Pharmaceuticals.药物合成中的绿色化学
Chem Rev. 2022 Feb 9;122(3):3637-3710. doi: 10.1021/acs.chemrev.1c00631. Epub 2021 Dec 15.
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Ultrasound-Assisted Iodination of Imidazo[1,2-α]pyridines Via C-H Functionalization Mediated by -Butyl Hydroperoxide.通过叔丁基过氧化氢介导的C-H官能化实现咪唑并[1,2-α]吡啶的超声辅助碘化反应
ACS Omega. 2021 Sep 28;6(40):25940-25949. doi: 10.1021/acsomega.1c02645. eCollection 2021 Oct 12.
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Imidazo[1,2-b]pyridazine as privileged scaffold in medicinal chemistry: An extensive review.咪唑并[1,2-b]哒嗪作为药物化学中的优势骨架：一篇广泛的综述。
Eur J Med Chem. 2021 Dec 15;226:113867. doi: 10.1016/j.ejmech.2021.113867. Epub 2021 Sep 23.