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第四代三步法粘结剂与第七代通用粘结剂界面断裂的比较研究

Comparative Study on Interface Fracture of 4th Generation 3-Steps Adhesive and 7th Generation Universal Adhesive.

作者信息

Călinoiu Ștefan George, Bîcleșanu Cornelia, Florescu Anamaria, Stoia Dan Ioan, Dumitru Cătălin, Miculescu Marian

机构信息

Doctoral School of Dentistry, Organizing Institution of University Doctoral Studies, "Titu Maiorescu" University, 67A Gh. Petrascu Street, 040441 Bucharest, Romania.

Faculty of Dental Medicine, "Titu Maiorescu" University, 67A Gh. Petrascu Street, 040441 Bucharest, Romania.

出版信息

Materials (Basel). 2023 Aug 25;16(17):5834. doi: 10.3390/ma16175834.

Abstract

The purpose of this paper is to compare the fracture behavior of interfaces obtained using fourth-generation and universal dental adhesives. The study relies on optic and SEM to evaluate the dentin-adhesive-restoration material interface of the samples and also on FEA simulation of fracture behavior. Specimen fabrication relied on 20 extracted teeth, in which class I cavities were created according to a protocol established based on the rules of minimally invasive therapy. For the direct adhesive technique, the adhesives used were: three-step All Bond, three-batch A and one-step Clearfil Universal Bond Quick-batch B. The restoration was performed with the same composite for both adhesives: Gradia direct posterior. The simulation used a 3D reconstructed molar on which geometric operations were performed to obtain an assembly that replicated a physical specimen. Material properties were applied to each component based on the information found in the literature. A simplified model for crack propagation was constructed, and using the fracture mechanics tool in Ansys 2019, the stress intensity factors that act at the crack tip of the adhesive interface were obtained. Mechanical simulation and microscopic investigation showed us how the interface of the dentine-adhesive-filling material performed in cases of both dental adhesives and for a certain loading condition. Important differences were identified among the adhesives, the fourth generation being superior to the fourth generation especially due to the separate steps in which the tooth surface was prepared for adhesion.

摘要

本文的目的是比较使用第四代牙科粘合剂和通用牙科粘合剂获得的界面的断裂行为。该研究依靠光学显微镜和扫描电子显微镜来评估样品的牙本质-粘合剂-修复材料界面,还依靠断裂行为的有限元分析模拟。样本制备依赖于20颗拔除的牙齿,其中I类洞按照基于微创治疗规则建立的方案制备。对于直接粘结技术,使用的粘合剂有:三步法全粘结剂、三批次A粘结剂和一步法Clearfil通用粘结快速批次B粘结剂。两种粘合剂的修复均使用相同的复合材料:Gradia直接后牙复合材料。模拟使用了一个三维重建的磨牙,在其上进行几何操作以获得一个复制物理样本的组件。根据文献中的信息将材料特性应用于每个组件。构建了一个简化的裂纹扩展模型,并使用Ansys 2019中的断裂力学工具,获得了作用于粘合剂界面裂纹尖端的应力强度因子。力学模拟和微观研究向我们展示了在两种牙科粘合剂以及特定加载条件下牙本质-粘合剂-填充材料的界面表现。在粘合剂之间发现了重要差异,第四代粘合剂尤其优于通用粘合剂,特别是由于在为粘结准备牙面时采用了分开的步骤。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ef9e/10488864/b61c02db6fc7/materials-16-05834-g001.jpg

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