Liu Yunqing, Sakaguchi Norihito, Iijima Masahiro, Islam Md Refat Readul, Zhang Jiayuan, Islam Rafiqul, Yamauti Monica, Sano Hidehiko, Tomokiyo Atsushi
Department of Restorative Dentistry, Faculty of Dental Medicine, Hokkaido University, Sapporo 0608586, Japan.
Center for Advanced Research of Energy Technology, Faculty of Engineering, Hokkaido University, Sapporo 0608628, Japan.
Polymers (Basel). 2023 Oct 5;15(19):3995. doi: 10.3390/polym15193995.
This study evaluated the effect of a 0.5% chloramine T solution on a chemical-cured universal adhesive by comparing the light-cured, one-step, self-etch adhesive for the bonding performance, mechanical properties, and resin-dentin interfacial characteristics. Caries-free human molars were randomly assigned into eight groups based on the bonding systems employed (Bond Force II, BF and Bondmer Lightless, BL), the immersion solutions used before bonding (0.5% chloramine T solution and distilled water), and the immersion durations (5 and 60 min). Microtensile bond strength (μTBS), nanoleakage evaluation, and nanoindentation tests were performed, and the surface morphology of the resin-dentin interface was examined using a focus ion beam/scanning ion microscopy system. Immersion in chloramine-T for 5 min significantly decreased the μTBS of Bondmer Lightless (from 22.62 to 12.87 MPa) compared with that in distilled water. Moreover, there was also a decreasing trend after immersing in chloramine-T for 60 min (from 19.11 to 13.93 MPa). Chloramine T was found to have no effect on the hardness, elastic modulus, or morphological characteristics of the ion-beam milled resin-dentin interfacial surfaces in the tested adhesives, suggesting that chloramine T might reduce the bond strength by interfering with the interaction and the sealing between the adhesive resin and dentin in the chemical-cured universal adhesive, albeit without affecting the mechanical properties.
本研究通过比较光固化一步自酸蚀粘结剂,评估了0.5%氯胺T溶液对化学固化通用粘结剂的粘结性能、机械性能和树脂-牙本质界面特性的影响。将无龋的人磨牙根据所采用的粘结系统(Bond Force II,BF和Bondmer Lightless,BL)、粘结前使用的浸泡溶液(0.5%氯胺T溶液和蒸馏水)以及浸泡时间(5分钟和60分钟)随机分为八组。进行了微拉伸粘结强度(μTBS)、纳米渗漏评估和纳米压痕测试,并使用聚焦离子束/扫描离子显微镜系统检查了树脂-牙本质界面的表面形态。与在蒸馏水中浸泡相比,在氯胺T中浸泡5分钟显著降低了Bondmer Lightless的μTBS(从22.62 MPa降至12.87 MPa)。此外,在氯胺T中浸泡60分钟后也有下降趋势(从19.11 MPa降至13.93 MPa)。研究发现,氯胺T对测试粘结剂中离子束研磨的树脂-牙本质界面表面的硬度、弹性模量或形态特征没有影响,这表明氯胺T可能通过干扰化学固化通用粘结剂中粘结树脂与牙本质之间的相互作用和密封来降低粘结强度,尽管不会影响机械性能。