Radhika N, Krishna S Aravind, Basak Animesh Kumar, Adediran Adeolu Adesoji
Department of Mechanical Engineering, Amrita School of Engineering, Amrita Vishwa Vidyapeetham, Coimbatore, India.
Adelaide Microscopy, The University of Adelaide, Adelaide, SA, Australia.
Sci Rep. 2024 Feb 13;14(1):3662. doi: 10.1038/s41598-024-54267-7.
Surface modification by suitable technique aids in improving the characteristics of material to resist severe wear in demanding environments and challenging applications. The present study aims to analyse the tribological performance of Stainless Steel (SS304) reinforced with CoCrCuFeTi High Entropy Alloy (HEA) through friction stir processing and compares the results with annealed specimens. The CoCrCuFeTi HEA was ball milled and revealed irregular fragment particles with Body Centred Cubic (BCC) phase. The processed samples exhibited excellent refinement in grains with uniform HEA reinforcement distribution. The grains were observed to be in nano level post-annealing promoting exceptional microhardness. The pin-on-disc wear test was conducted by varying load (10-40N), sliding velocity (0.5-3.5 m/s) and sliding distance (500-2000 m) and the respective worn surface was analysed. The processed sample with HEA after annealing offered 29.8%, 57.4% and 58.49% improved wear resistance at the minimum level of load, sliding velocity and sliding distance than the processed base samples. The worn morphology revealed delamination, abrasion, adhesion and oxide layer formation to be the predominant wear mechanisms.
通过合适的技术进行表面改性有助于改善材料的特性,使其在苛刻环境和具有挑战性的应用中抵抗严重磨损。本研究旨在通过搅拌摩擦加工分析钴铬铜铁钛高熵合金(HEA)增强不锈钢(SS304)的摩擦学性能,并将结果与退火试样进行比较。对钴铬铜铁钛高熵合金进行球磨后,发现其具有体心立方(BCC)相的不规则碎片颗粒。加工后的样品在晶粒细化方面表现出色,高熵合金增强相分布均匀。观察到退火后晶粒处于纳米级,从而具有优异的显微硬度。通过改变载荷(10 - 40N)、滑动速度(0.5 - 3.5 m/s)和滑动距离(500 - 2000 m)进行销盘磨损试验,并对相应的磨损表面进行分析。与加工后的基体样品相比,退火后的含高熵合金加工样品在最低载荷、滑动速度和滑动距离水平下的耐磨性分别提高了29.8%、57.4%和58.49%。磨损形态表明分层、磨损、粘着和氧化层形成是主要的磨损机制。