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用于原子力显微镜的磁电悬臂梁

Magnetic-Dielectric Cantilevers for Atomic Force Microscopy.

作者信息

Sanchez-Seguame Gala, Avalos-Sanchez Hugo, Eduardo Lugo Jesus, Murillo-Bracamontes Eduardo Antonio, Palomino-Ovando Martha Alicia, Hernández-Cristobal Orlando, Gervacio-Arciniega José Juan, Toledo-Solano Miller

机构信息

Facultad de Ciencias Físico-Matemáticas, Benemérita Universidad Autónoma de Puebla, Av. San Claudio y Av. 18 sur, Col. San Manuel Ciudad Universitaria, Puebla Pue 72570, Mexico.

Faubert Lab, School of Optometry, University of Montreal, Montreal, QC H3T1P1, Canada.

出版信息

Nanomaterials (Basel). 2024 May 17;14(10):874. doi: 10.3390/nano14100874.

Abstract

Atomic force microscopy (AFM) is a technique that relies on detecting forces at the nanonewton scale. It involves using a cantilever with a tiny tip at one end. This tip interacts with the short- and long-range forces of material surfaces. These cantilevers are typically manufactured with Si or SiN and synthesized using a lithography technique, which implies a high cost. On the other hand, through simple chemical methods, it is possible to synthesize a magneto-dielectric composite made up of artificial SiO opals infiltrated with superparamagnetic nanoparticles of FeO. From these materials, it is possible to obtain tipless cantilevers that can be used in AFM analysis. Tipless cantilevers are an alternative tool in nanoscale exploration, offering a versatile approach to surface analysis. Unlike traditional AFM probes, tipless versions eliminate the challenges associated with tip wear, ensuring prolonged stability during measurements. This makes tipless AFM particularly valuable for imaging delicate or soft samples, as it prevents sample damage and provides precise measurements of topography and mechanical and electromechanical properties. This study presents the results of the characterization of known surfaces using magneto-dielectric cantilevers and commercial cantilevers based on Si. The characterization will be carried out through contact and non-contact topography measurements.

摘要

原子力显微镜(AFM)是一种依靠检测纳牛顿尺度力的技术。它涉及使用一端带有微小尖端的悬臂。该尖端与材料表面的短程和长程力相互作用。这些悬臂通常由硅或氮化硅制造,并使用光刻技术合成,这意味着成本高昂。另一方面,通过简单的化学方法,可以合成一种磁电介质复合材料,该材料由渗透有超顺磁性FeO纳米颗粒的人造SiO蛋白石组成。从这些材料中,可以获得可用于AFM分析的无尖端悬臂。无尖端悬臂是纳米级探索中的一种替代工具,为表面分析提供了一种通用方法。与传统的AFM探针不同,无尖端版本消除了与尖端磨损相关的挑战,确保了测量过程中的长期稳定性。这使得无尖端AFM对于成像精细或柔软的样品特别有价值,因为它可以防止样品损坏,并提供精确的形貌以及机械和机电性能测量。本研究展示了使用磁电介质悬臂和基于硅的商业悬臂对已知表面进行表征的结果。表征将通过接触式和非接触式形貌测量来进行。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/ddb6/11123794/bce2f8c36159/nanomaterials-14-00874-g001.jpg

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