• 文献检索
  • 文档翻译
  • 深度研究
  • 学术资讯
  • Suppr Zotero 插件Zotero 插件
  • 邀请有礼
  • 套餐&价格
  • 历史记录
应用&插件
Suppr Zotero 插件Zotero 插件浏览器插件Mac 客户端Windows 客户端微信小程序
定价
高级版会员购买积分包购买API积分包
服务
文献检索文档翻译深度研究API 文档MCP 服务
关于我们
关于 Suppr公司介绍联系我们用户协议隐私条款
关注我们

Suppr 超能文献

核心技术专利:CN118964589B侵权必究
粤ICP备2023148730 号-1Suppr @ 2026

文献检索

告别复杂PubMed语法,用中文像聊天一样搜索,搜遍4000万医学文献。AI智能推荐,让科研检索更轻松。

立即免费搜索

文件翻译

保留排版,准确专业,支持PDF/Word/PPT等文件格式,支持 12+语言互译。

免费翻译文档

深度研究

AI帮你快速写综述,25分钟生成高质量综述,智能提取关键信息,辅助科研写作。

立即免费体验

选定生物材料中游离脂肪酸测定的综合研究:综述

A Comprehensive Study for Determination of Free Fatty Acids in Selected Biological Materials: A Review.

作者信息

Uçar Beyza, Gholami Zahra, Svobodová Kateřina, Hradecká Ivana, Hönig Vladimír

机构信息

ORLEN UniCRE a.s., Revoluční 1521/84, 400 01 Ústí nad Labem, Czech Republic.

Department of Chemistry, Faculty of Agrobiology, Food and Natural Resources, Czech University of Life Sciences Prague, Kamýcká 129, 165 00 Prague, Czech Republic.

出版信息

Foods. 2024 Jun 16;13(12):1891. doi: 10.3390/foods13121891.

DOI:10.3390/foods13121891
PMID:38928832
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC11203194/
Abstract

The quality of oil is highly dependent on its free fatty acid (FFA) content, especially due to increased restrictions on renewable fuels. As a result, there has been a growing interest in free fatty acid determination methods over the last few decades. While various standard methods are currently available, such as the American Oil Chemists Society (AOCS), International Union of Pure and Applied Chemistry (IUPAC), and Japan Oil Chemists' Society (JOCS), to obtain accurate results, there is a pressing need to investigate a fast, accurate, feasible, and eco-friendly methodology for determining FFA in biological materials. This is owing to inadequate characteristics of the methods, such as solvent consumption and reproducibility, among others. This study aims to investigate FFA determination methods to identify suitable approaches and introduce a fresh perspective.

摘要

油的质量高度依赖于其游离脂肪酸(FFA)含量,特别是由于对可再生燃料的限制日益增加。因此,在过去几十年里,人们对游离脂肪酸测定方法的兴趣与日俱增。虽然目前有各种标准方法,如美国油脂化学家协会(AOCS)、国际纯粹与应用化学联合会(IUPAC)和日本油脂化学家协会(JOCS),但为了获得准确的结果,迫切需要研究一种快速、准确、可行且环保的方法来测定生物材料中的游离脂肪酸。这是因为这些方法存在诸如溶剂消耗和重现性等不足之处。本研究旨在探究游离脂肪酸测定方法,以确定合适的方法并引入新的视角。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/3d58599cf3ca/foods-13-01891-g014.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/88aa9e242b31/foods-13-01891-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/d73871875eed/foods-13-01891-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/dee18806e596/foods-13-01891-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/58d720e41575/foods-13-01891-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/855afcd206bb/foods-13-01891-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/d3b7a01ecf1f/foods-13-01891-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/111a76279dc5/foods-13-01891-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/3521d3ff64a0/foods-13-01891-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/78d9920081ae/foods-13-01891-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/5132bf59df47/foods-13-01891-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/906cd7bb3d08/foods-13-01891-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/f1b13289e563/foods-13-01891-g012.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/248bf0bd8dc4/foods-13-01891-g013.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/3d58599cf3ca/foods-13-01891-g014.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/88aa9e242b31/foods-13-01891-g001.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/d73871875eed/foods-13-01891-g002.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/dee18806e596/foods-13-01891-g003.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/58d720e41575/foods-13-01891-g004.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/855afcd206bb/foods-13-01891-g005.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/d3b7a01ecf1f/foods-13-01891-g006.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/111a76279dc5/foods-13-01891-g007.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/3521d3ff64a0/foods-13-01891-g008.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/78d9920081ae/foods-13-01891-g009.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/5132bf59df47/foods-13-01891-g010.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/906cd7bb3d08/foods-13-01891-g011.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/f1b13289e563/foods-13-01891-g012.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/248bf0bd8dc4/foods-13-01891-g013.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/3493/11203194/3d58599cf3ca/foods-13-01891-g014.jpg

相似文献

1
A Comprehensive Study for Determination of Free Fatty Acids in Selected Biological Materials: A Review.选定生物材料中游离脂肪酸测定的综合研究:综述
Foods. 2024 Jun 16;13(12):1891. doi: 10.3390/foods13121891.
2
An indirect analytical approach based on ATR-FTIR spectroscopy for determining the FFA content in vegetable oils.一种基于衰减全反射傅里叶变换红外光谱法测定植物油中游离脂肪酸含量的间接分析方法。
RSC Adv. 2020 Jun 24;10(40):24073-24078. doi: 10.1039/d0ra03668d. eCollection 2020 Jun 19.
3
Environmentally friendly processes from coffee wastes to trimethylolpropane esters to be considered biolubricants.考虑将咖啡废料转化为三羟甲基丙烷酯的环保工艺作为生物润滑剂。
J Air Waste Manag Assoc. 2020 Nov;70(11):1198-1215. doi: 10.1080/10962247.2020.1788664. Epub 2020 Oct 1.
4
Rapid determination of total trans fat content--an attenuated total reflection infrared spectroscopy international collaborative study.总反式脂肪含量的快速测定——衰减全反射红外光谱国际协作研究
J AOAC Int. 2001 Jul-Aug;84(4):1144-50.
5
Rapid determination of free fatty acids in poultry feed lipid extracts by SB-ATR FTIR spectroscopy.通过衰减全反射傅里叶变换红外光谱法快速测定家禽饲料脂质提取物中的游离脂肪酸
J Agric Food Chem. 2007 Jun 27;55(13):4928-32. doi: 10.1021/jf063554f. Epub 2007 May 26.
6
Rapid determination of free fatty acid content in waste deodorizer distillates using single bounce-attenuated total reflectance-FTIR spectroscopy.使用单反射衰减全反射傅里叶变换红外光谱法快速测定废除臭剂馏出物中的游离脂肪酸含量。
J AOAC Int. 2012 Nov-Dec;95(6):1570-3. doi: 10.5740/jaoacint.11-034.
7
Validation of the Free Fatty Acid Test Kit for the Measurement of the Free Fatty Acid Content of Vegetable Oils, Fish Oils, Animal Fats (Tallows), Meat and Fish Meals, and Potato Chips and Grain-Based Snack Products: AOAC Performance Tested MethodSM 052004.油脂游离脂肪酸测试试剂盒测定植物油、鱼油、动物脂肪(牛脂)、肉和鱼粉、薯片和谷物类小吃游离脂肪酸含量的验证:AOAC 性能验证方法标准 052004。
J AOAC Int. 2021 May 21;104(2):300-311. doi: 10.1093/jaoacint/qsaa086.
8
Determination of trans unsaturation by infrared spectrophotometry and determination of fatty acid composition of partially hydrogenated vegetable oils and animal fats by gas chromatography/infrared spectrophotometry: collaborative study.用红外分光光度法测定反式不饱和度以及用气相色谱法/红外分光光度法测定部分氢化植物油和动物脂肪的脂肪酸组成:协同研究
J AOAC Int. 1995 May-Jun;78(3):783-802.
9
Profile of trans fatty acids (FAs) including trans polyunsaturated FAs in representative fast food samples.代表性快餐样品中反式脂肪酸(FAs)的概况,包括反式多不饱和 FAs。
J Agric Food Chem. 2012 May 9;60(18):4567-77. doi: 10.1021/jf300585s. Epub 2012 Apr 26.
10
Improved determination of isolated trans isomers in edible oils by Fourier transform infrared spectroscopy using spectral reconstitution.利用光谱重构的傅里叶变换红外光谱法改进食用油中分离反式异构体的测定
J AOAC Int. 2007 Mar-Apr;90(2):446-51.

引用本文的文献

1
Sustainable biodiesel production from cottonseed oil using a nickel-doped eggshell heterogeneous catalyst optimized via response surface methodology.使用通过响应面法优化的镍掺杂蛋壳非均相催化剂从棉籽油中可持续生产生物柴油。
Sci Rep. 2025 Sep 1;15(1):32132. doi: 10.1038/s41598-025-17529-6.
2
The Effect of Grape Seed Extract on Lipid Oxidation, Color Change, and Microbial Growth in a Beef-Pork Sausage Model System.葡萄籽提取物对牛肉-猪肉香肠模型体系中脂质氧化、颜色变化及微生物生长的影响
Molecules. 2025 Apr 13;30(8):1739. doi: 10.3390/molecules30081739.
3
Comprehensive quantification of C4 to C26 free fatty acids using a supercritical fluid chromatography-mass spectrometry method in pharmaceutical-grade egg yolk powders intended for total parenteral nutrition use.

本文引用的文献

1
Fabrication of immobilized lipases from on hierarchical mesoporous silica for enzymatic enrichment of ω-3 polyunsaturated fatty acids by selective hydrolysis.基于分级介孔二氧化硅固定化脂肪酶的制备及其通过选择性水解对ω-3多不饱和脂肪酸进行酶法富集
Food Chem X. 2024 May 10;22:101434. doi: 10.1016/j.fochx.2024.101434. eCollection 2024 Jun 30.
2
A digital image-based colorimetric method for measuring free acidity in edible vegetable oils.基于数字图像的食用植物油游离酸度比色测定方法。
Food Chem. 2024 Jun 15;443:138555. doi: 10.1016/j.foodchem.2024.138555. Epub 2024 Jan 24.
3
Optimization of HPLCCAD method for simultaneous analysis of different lipids in lipid nanoparticles with analytical QbD.
使用超临界流体色谱-质谱法对用于全胃肠外营养的药用级蛋黄粉中C4至C26游离脂肪酸进行全面定量分析。
Anal Bioanal Chem. 2025 Mar;417(8):1461-1478. doi: 10.1007/s00216-025-05732-3. Epub 2025 Jan 23.
采用分析 QbD 对脂质纳米粒中不同脂质进行高效液相色谱-串联质谱同时分析方法的优化。
J Chromatogr A. 2023 Oct 25;1709:464375. doi: 10.1016/j.chroma.2023.464375. Epub 2023 Sep 16.
4
A comparative evaluation of low-field and high-field NMR untargeted analysis: Authentication of virgin coconut oil adulterated with refined coconut oil as a case study.低场和高场 NMR 非靶向分析的比较评估:以 virgin coconut oil 掺 refined coconut oil 为例进行掺假鉴定。
Anal Chim Acta. 2023 Sep 8;1273:341537. doi: 10.1016/j.aca.2023.341537. Epub 2023 Jun 21.
5
Influence of free fatty acid content and degree of fat saturation on production performance, nutrient digestibility, and intestinal morphology of laying hens.游离脂肪酸含量和脂肪饱和度对蛋鸡生产性能、养分消化率及肠道形态的影响
Anim Nutr. 2023 Mar 28;13:313-323. doi: 10.1016/j.aninu.2023.03.002. eCollection 2023 Jun.
6
Spectroscopic studies on thermal degradation and quantitative prediction on acid value of edible oil during frying by Raman spectroscopy.拉曼光谱法研究食用油在煎炸过程中的热降解及酸值的定量预测。
Spectrochim Acta A Mol Biomol Spectrosc. 2023 May 15;293:122477. doi: 10.1016/j.saa.2023.122477. Epub 2023 Feb 10.
7
Recent progress in the analysis of unsaturated fatty acids in biological samples by chemical derivatization-based chromatography-mass spectrometry methods.基于化学衍生化的色谱-质谱法分析生物样品中不饱和脂肪酸的最新进展。
J Chromatogr B Analyt Technol Biomed Life Sci. 2023 Jan 15;1215:123572. doi: 10.1016/j.jchromb.2022.123572. Epub 2022 Dec 15.
8
Chemometric analysis applied to H NMR and FTIR data for a quality parameter distinction of red fruit (Pandanus conoideus, lam.) oil products.化学计量学分析应用于红果(露兜树属圆锥叶露兜树,Lam.)油产品质量参数区分的氢核磁共振和傅里叶变换红外光谱数据。
Phytochem Anal. 2023 Oct;34(7):788-799. doi: 10.1002/pca.3196. Epub 2022 Dec 12.
9
Life Cycle Greenhouse Gas Emissions of Biodiesel and Renewable Diesel Production in the United States.美国生物柴油和可再生柴油生产的生命周期温室气体排放。
Environ Sci Technol. 2022 Jun 21;56(12):7512-7521. doi: 10.1021/acs.est.2c00289. Epub 2022 May 16.
10
Application of H NMR in the study of fatty acids composition of vegetable oils.NMR 在植物油脂肪酸组成研究中的应用。
J Pharm Biomed Anal. 2022 Apr 1;212:114658. doi: 10.1016/j.jpba.2022.114658. Epub 2022 Feb 10.