Improved benchtop P NMR reaction monitoring Multi-Resonance SHARPER.
作者信息
Tadiello Laura, Halse Meghan E, Beweries Torsten
机构信息
Leibniz Institute for Catalysis (LIKAT), Albert-Einstein-Str. 29a, 18059 Rostock, Germany.
Department of Chemistry, University of York, YO10 5DD, York, UK.
出版信息
Anal Methods. 2024 Aug 8;16(31):5399-5402. doi: 10.1039/d4ay00948g.
PMID:39042022
Abstract
reaction monitoring of hydrogenation reactions featuring oxygen-sensitive organometallic complexes is done a P benchtop NMR spectrometer using the Multi-Resonance Sensitive Homogeneous And Resolved PEaks in Real time (MR-SHARPER) sequence. Signal enhancement generated by MR-SHARPER enables monitoring of reactivity on the order of minutes that could not be followed with traditional P{H} NMR detection.
摘要
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