Tosun Büşra, Öztürk Zeynep, Uysal Nur
Department of Prosthodontics, Faculty of Dentistry, University of Abant İzzet Baysal, 14030 Bolu, Turkey.
Department of Pedodontics, Faculty of Dentistry, University of Abant İzzet Baysal, 14030 Bolu, Turkey.
Polymers (Basel). 2024 Dec 29;17(1):56. doi: 10.3390/polym17010056.
This study evaluated the color stability, surface roughness, and hardness of 3D-printed and heat-polymerized denture materials. A total of 90 samples were prepared, with equal numbers of 3D-printed and heat-polymerized disks. The initial hardness, surface roughness, and color values of the samples were measured. After 14 days of immersion in distilled water, natural orange juice, or commercial orange juice, the measurements were repeated. Based on the findings, 3D-printed samples exhibited a greater reduction in Vickers hardness (56.24 ± 15.81%) compared to heat-polymerized samples (18.93 ± 11.41%). Materials immersed in commercial orange juice exhibited a greater reduction in hardness compared to those in other solutions (43.13 ± 23.66). Surface roughness increased by 46.66 ± 26.8% in heat-polymerized samples and by 26.16 ± 20.78% in 3D-printed samples, with the highest increase observed in commercial orange juice (50.73 ± 28.8%) ( < 0.001). The color change (ΔE) was significantly higher in heat-polymerized samples (ΔE = 5.05 ± 0.28) than in 3D-printed samples (ΔE = 3.9 ± 0.26) ( < 0.001). This study demonstrates that the material type and immersion solutions play a critical role in determining the mechanical and optical properties of denture materials, with commercial orange juice having the most pronounced effect on surface roughness and hardness.
本研究评估了3D打印和热聚合义齿材料的颜色稳定性、表面粗糙度和硬度。共制备了90个样本,3D打印和热聚合圆盘数量相等。测量了样本的初始硬度、表面粗糙度和颜色值。将样本在蒸馏水、天然橙汁或市售橙汁中浸泡14天后,重复进行测量。根据研究结果,与热聚合样本(18.93±11.41%)相比,3D打印样本的维氏硬度降低幅度更大(56.24±15.81%)。与其他溶液中的材料相比,浸泡在市售橙汁中的材料硬度降低幅度更大(43.13±23.66)。热聚合样本的表面粗糙度增加了46.66±26.8%,3D打印样本增加了26.16±20.78%,在市售橙汁中增加幅度最高(50.73±28.8%)(<0.001)。热聚合样本的颜色变化(ΔE)显著高于3D打印样本(ΔE=5.05±0.28)(ΔE=3.9±0.26)(<0.001)。本研究表明,材料类型和浸泡溶液在决定义齿材料的机械和光学性能方面起着关键作用,市售橙汁对表面粗糙度和硬度的影响最为显著。