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高效液相色谱法测定FD&C黄6号中的4,4'-(重氮氨基)二苯磺酸

High pressure liquid chromatographic determination of 4,4'-(diazoamino)-dibenzenesulfonic acid in FD&C yellow no. 6.

作者信息

Marmion D M

出版信息

J Assoc Off Anal Chem. 1977 Jan;60(1):168-72.

PMID:401804
Abstract

Fourteen analysts from 9 laboratories evaluated a high pressure liquid chromatographic procedure for the determination of 4,4'-(diazoamino)-dibenzenesulfonic acid (DAADBSA) in FD&C Yellow No. 6. Each collaborator analyzed 5 samples nominally containing 0-0.050% DAADBSA. The repeatability and reproducibility of the method are estimated to be 0.003% and 0.020%, respectively. The method has been adopted as offical fist action.

摘要

来自9个实验室的14名分析人员对一种用于测定FD&C黄6号中4,4'-(重氮氨基)二苯磺酸(DAADBSA)的高压液相色谱法进行了评估。每位协作人员分析了5个标称含有0-0.050% DAADBSA的样品。该方法的重复性和再现性估计分别为0.003%和0.020%。该方法已被采用为官方首次行动方法。

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