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胃酸侵蚀试验:牙齿颜色修复材料的机械性能和表面光泽度。

Gastric acid challenge: Mechanical proficiency and surface gloss of tooth-colored restorative materials.

作者信息

Yenidunya Ozge Gizem, Misilli Tugba, Yilmaz Ebru

机构信息

Department of Restorative Dentistry, Faculty of Dentistry, Pamukkale University, Denizli, 20160, Turkey.

Department of Restorative Dentistry, Faculty of Dentistry, Çanakkale Onsekiz Mart University, 17100, Çanakkale, Turkey.

出版信息

BMC Oral Health. 2025 Apr 21;25(1):614. doi: 10.1186/s12903-025-05988-2.

Abstract

BACKGROUND

To evaluate surface microhardness, roughness, and gloss changes of tooth-colored restorative materials [a direct composite (G-aenial A'Chord), an indirect composite (Gradia Plus), an ormocer (Admira Fusion), a giomer (Beautifil II), and an alkasite (Cention N)] after exposure to simulated gastric acid.

METHODS

A total of 110 disc-shaped specimens (22 discs of each material) were prepared using silicone molds (8 mm×2 mm) and exposed to either gastric acid or artificial saliva (control). Surface roughness (Ra), gloss (GU), and microhardness (VHN) were measured at baseline and after 96-hour of immersion in the solutions and the respective changes (∆Ra, ∆GU, ∆VHN) were calculated. Intergroup comparisons were performed using ANOVA (Tukey post hoc) or Kruskal-Wallis tests (Bonferroni correction). Independent samples t-test or Mann-Whitney U test was used for comparisons of each material across immersion media, while paired t-test was applied for time-dependent analyses.

RESULTS

In the gastric acid medium, changes in all parameters led to significant differences among restorative materials, while in the artificial saliva medium, significant differences were observed in ∆VHN and ∆GU. The statistically significant difference between immersion media was observed in both ∆VHN and ∆Ra values for the giomer group, and in only ∆VHN values for the alkasite and indirect composite groups. In the gastric acid medium, the decrease in VHN and GU values was significant across all subgroups, while the increase in Ra was statistically significant only in the giomer and alkasite groups.

CONCLUSIONS

While the giomer group exhibited the most significant changes in roughness and microhardness following exposure to gastric acid, all tested materials executed clinically admissible results regarding surface gloss.

CLINICAL TRIAL NUMBER

Not applicable.

摘要

背景

评估牙齿颜色修复材料(一种直接复合树脂材料(G-aenial A'Chord)、一种间接复合树脂材料(Gradia Plus)、一种有机陶瓷(Admira Fusion)、一种聚酸改性复合树脂(Beautifil II)和一种碱硅酸玻璃离子(Cention N))在暴露于模拟胃酸后的表面显微硬度、粗糙度和光泽度变化。

方法

使用硅树脂模具(8毫米×2毫米)制备总共110个圆盘形试件(每种材料22个圆盘),并将其暴露于胃酸或人工唾液(对照)中。在基线以及在溶液中浸泡96小时后测量表面粗糙度(Ra)、光泽度(GU)和显微硬度(VHN),并计算各自的变化(∆Ra、∆GU、∆VHN)。使用方差分析(Tukey事后检验)或Kruskal-Wallis检验(Bonferroni校正)进行组间比较。独立样本t检验或Mann-Whitney U检验用于比较每种材料在不同浸泡介质中的情况,而配对t检验用于时间依赖性分析。

结果

在胃酸介质中,所有参数的变化导致修复材料之间存在显著差异,而在人工唾液介质中,∆VHN和∆GU中观察到显著差异。聚酸改性复合树脂组在∆VHN和∆Ra值方面,以及碱硅酸玻璃离子组和间接复合树脂组仅在∆VHN值方面,观察到浸泡介质之间存在统计学显著差异。在胃酸介质中,所有亚组的VHN和GU值均显著降低,而Ra的增加仅在聚酸改性复合树脂组和碱硅酸玻璃离子组中具有统计学显著性。

结论

虽然聚酸改性复合树脂组在暴露于胃酸后粗糙度和显微硬度变化最为显著,但所有测试材料在表面光泽度方面均取得了临床可接受的结果。

临床试验编号

不适用。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/928a/12012973/3ff326cd8c7c/12903_2025_5988_Fig1_HTML.jpg

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