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Detection of low-level carbadox residues in animal feeds by high pressure liquid chromatography.

作者信息

Luchtefeld R G

出版信息

J Assoc Off Anal Chem. 1977 Mar;60(2):279-83.

PMID:557035
Abstract

The high pressure liquid chromatographic (HPLC) method is capable of detecting from 1 to 0.024 ppm methyl 3-(2-quinoxalinyl-methylene)carbazate-N1,N4-dioxide (carbadox). Carbadox is extracted from the feed with 2% NH4OH in acetone, passed through a liquid-liquid partition, subjected to HPLC, and detected by using a 365 nm detector. No feed materials or other active drug ingredients produced false positive results.

摘要

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