Davis N D, Guy M L, Diener U L
J Assoc Off Anal Chem. 1981 Sep;64(5):1974-6.
Several innovations in the fluorometric-iodine (FL-I) method for determining aflatoxin in corn made the procedure faster and more convenient than the original method. Ground corn was packed into a chromatographic column and the aflatoxins were extracted with methylene chloride. Sep-Pak C18 cartridges were used for sample cleanup. A 5 min thin layer chromatographic slide analysis confirmed the presence of aflatoxin, which was quantitated by fluorometric determinations of the iodine derivative of aflatoxin B1.
用于测定玉米中黄曲霉毒素的荧光碘（FL-I）法的多项创新使该方法比原始方法更快、更便捷。将磨碎的玉米装入色谱柱，用二氯甲烷提取黄曲霉毒素。使用Sep-Pak C18柱进行样品净化。通过5分钟的薄层色谱玻片分析确认黄曲霉毒素的存在，然后通过对黄曲霉毒素B1碘衍生物的荧光测定进行定量。
