伊波加因生物碱的高效液相色谱法。I. 反相分离
High-performance liquid chromatography of eburnane alkaloids. I. Separation on reversed phases.
作者信息
Szepesi G, Gazdag M
出版信息
J Chromatogr. 1981 Jan 16;204:341-8. doi: 10.1016/s0021-9673(00)81677-5.
PMID:7217263
Abstract
Separation of eburnane alkaloids using reversed-phase high-performance liquid chromatography was investigated on muBondapak C18 in LiChrosorb RP-8 columns with acetonitrile-aqueous 0.01 M ammonium carbonate as eluent. The method can be successfully applied for the group separation of eburnane alkaloids as well as for the separation of stereoisomers and of ester homologues.
摘要
研究了在μBondapak C18和LiChrosorb RP - 8柱上，以乙腈 - 0.01M碳酸铵水溶液为洗脱剂，使用反相高效液相色谱法分离乌檀烷生物碱。该方法可成功应用于乌檀烷生物碱的分组分离以及立体异构体和酯同系物的分离。
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