3-表蜕皮激素和3-表-20-羟基蜕皮激素的制备。
Preparation of 3-epi-ecdysone and 3-epi-20-hydroxyecdysone.
作者信息
Dinan L, Rees H H
出版信息
Steroids. 1978 Dec;32(5):629-38. doi: 10.1016/0039-128x(78)90073-9.
PMID:734697
Abstract
3-Dehydro-ecdysone and 3-dehydro-20-hydroxyecdysone were prepared and characterized. Reduction of these compounds with NaBH4 gave 3-epi-ecdysone and 3-epi-20-hydroxyecdysone, which were characterized fully by mass and p.m.r. spectrometry as well as by derivative formation.
摘要
制备并表征了3-脱氢蜕皮激素和3-脱氢-20-羟基蜕皮激素。用硼氢化钠还原这些化合物得到3-表蜕皮激素和3-表-20-羟基蜕皮激素，通过质谱、核磁共振光谱以及衍生物的形成对其进行了全面表征。
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