Kim K H, Park J H, Imai Y, Kishi T
Department of Dental Materials, Dental College, Kyungpook National University, Dong-in Dong, Taegu, Korea.
J Dent Res. 1994 Feb;73(2):499-504. doi: 10.1177/00220345940730020301.
The effects of spherically-shaped filler particles on bending strength, bending elastic modulus, and fracture toughness of resin composites were studied. The filler content was changed by 0, 20, 40, 60, and 70 wt%. Bending properties and fracture toughnesses were determined on three-point bending specimens. Acoustic Emission (AE), i.e., the elastic wave released from a localized source in the material, was detected by sensors of a high-sensitivity and low-noise resonance type during the fracture toughness test. Detected acoustic emission signals were analyzed for parameters such as amplitude, events, and locations. The fractured surface was examined by a scanning electron microscope. The bending strength and the fracture toughness showed almost the same trend in their increasing rates by filler content, but the elastic modulus showed a much higher increasing rate. A microfracture mechanism of the dental resin composites containing spherically-shaped filler particles is proposed based on the results obtained from the AE-releasing pattern, two-dimensional AE location, and fracture surface findings. In addition to the toughening effects of crack pinning and crack branching, which are observed in the usual commercial resin composites, crack-deflecting effects are confirmed in this new type of dental resin composites.
研究了球形填料颗粒对树脂复合材料弯曲强度、弯曲弹性模量和断裂韧性的影响。填料含量分别为0、20、40、60和70 wt%。在三点弯曲试样上测定弯曲性能和断裂韧性。在断裂韧性试验期间,通过高灵敏度、低噪声共振型传感器检测声发射(AE),即材料中局部源释放的弹性波。对检测到的声发射信号进行幅度、事件和位置等参数分析。用扫描电子显微镜检查断裂表面。弯曲强度和断裂韧性随填料含量的增加速率几乎相同,但弹性模量的增加速率要高得多。基于从声发射释放模式、二维声发射定位和断裂表面观察结果获得的结果,提出了含球形填料颗粒的牙科树脂复合材料的微断裂机制。除了在普通商业树脂复合材料中观察到的裂纹钉扎和裂纹分支增韧效应外,在这种新型牙科树脂复合材料中还证实了裂纹偏转效应。