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牙科修复材料的断裂韧性。

Fracture toughness of dental restorative materials.

机构信息

Department of Restorative Dentistry, Dental School of the Ludwig-Maximilians-University, Goethestr. 70, Munich 80336, Germany.

出版信息

Clin Oral Investig. 2012 Apr;16(2):489-98. doi: 10.1007/s00784-011-0525-z. Epub 2011 Mar 2.

Abstract

The ability of a restorative material to withstand fracture is of crucial importance especially in stress-bearing area. Therefore, the study aims to analyse the fracture toughness of a large number of dental restorative materials categories. The fracture toughness (K(IC)) of 69 restorative materials belonging to ten materials categories-micro-hybrid, nanofilled, microfilled, packable, ormocer-based, and flowable resin-based composites (RBC), compomers and flowable compomers, as well as glass ionomer cements (GIC) and resin-modified GIC was measured by means of the single-edge notched-beam method after storing the samples (n = 8) for 24 h in distilled water. Data were analyzed with the one-way analysis of variance (ANOVA) followed by the Tukey's test and partial eta-squared statistics (p < 0.05). Large variations between the tested materials within a material category were found. The lowest fracture toughness was reached in the GIC group, followed by the microfilled RBCs, resin-modified GIC, and flowable compomers, which do not differ significantly among each other as a material group. The ormocer-based, packable, and micro-hybrid RBCs performed statistically similar, reaching the highest fracture toughness values. Between the two categories of flowables-composites and compomers-no differences were measured. The correlation between K(IC) and filler volume (0.34) and respective filler weight (0.40) was low. K(IC) increased with the volume fraction of fillers until a critical value of 57%, following with a plateau, with constant values until ca. 65% volume fraction. Above this value, K(IC) decreased slightly. Due to the very large variability of the fracture toughness within a material type, the selection of a suitable restorative material should have not been done with respect to a specific material category, especially in stress-bearing areas, but by considering the individual measured material properties.

摘要

修复材料的抗断裂能力尤为重要,特别是在承重区域。因此,本研究旨在分析大量不同种类的牙科修复材料的断裂韧性。通过单边切口梁法对 10 种材料类别中的 69 种修复材料(包括微混合、纳米填充、微填充、可填充、有机陶瓷基和流动性树脂基复合材料、复合体和流动性复合体、玻璃离聚物水泥和树脂改性玻璃离聚物水泥)的断裂韧性(K(IC))进行测量。将样本(n=8)在蒸馏水中储存 24 小时后,使用单边切口梁法对样本进行测量。采用单因素方差分析(ANOVA)对数据进行分析,然后采用 Tukey 检验和偏 eta-平方统计(p<0.05)。发现同一材料类别内测试材料之间存在较大差异。GIC 组的断裂韧性最低,其次是微填充 RBC、树脂改性 GIC 和流动性复合体,它们作为一个材料组之间没有显著差异。有机陶瓷基、可填充和微混合 RBC 的性能相似,达到了最高的断裂韧性值。在两种流动性复合材料和复合体类别之间没有差异。K(IC)与填料体积(0.34)和相应填料重量(0.40)之间的相关性较低。K(IC)随着填料体积分数的增加而增加,直到达到 57%的临界值,随后进入一个平台,直到约 65%的体积分数,保持恒定值。超过这个值后,K(IC)略有下降。由于材料类型内断裂韧性的变化很大,因此,在选择合适的修复材料时,不应根据特定的材料类别来选择,特别是在承重区域,而应考虑个别测量的材料特性。

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