Gwinnett A J
Department of Oral Biology & Pathology, SUNY at Stony Brook, Stony Brook, NY 11794.
Am J Dent. 1993 Feb;6(1):7-9.
This study determined, quantitatively, the role of resin infiltration in dentin bonding. Four groups contained 10 molar teeth. Thirty were sectioned in the mid-coronal region and the dentin ground flat with 600 grit silicon carbide paper. Group 1: smear layer intact; Group 2: smear layer removed with a Prophy Jet; Group 3: conditioned with 10% H3PO4 for 20 seconds; Group 4: comprised dentin exposed by a transverse, mid-coronal fracture. Dentin surfaces were treated with All-Bond 2, its companion bonding agent, followed by P50 resin composite, polymerized in 1 mm increments. After storage in water at 37 degrees C for 24 hours, the assemblies were tested to failure in a shear mode at a crosshead speed of 5 mm/minute. Surface and interfacial morphology was characterized using SEM. Values in MPa were: Group 1: 10.24 +/- 2.98; Group 2: 20.37 +/- 4.62; Group 3: 32.68 +/- 7.12; and Group 4: 26.77 +/- 4.85. ANOVA and student t-test showed the means statistically different (P < 0.05). Since resin penetration was only found appreciably in dentin tubules in Group 4 and tubular and intertubular penetration in Group 3, it was concluded that resin infiltration can contribute approximately one third of the shear bond strength of this total etch system.
本研究定量确定了树脂渗透在牙本质粘结中的作用。四组各含10颗磨牙。将30颗牙齿在牙冠中部区域进行切片,并用600目碳化硅砂纸将牙本质磨平。第1组:玷污层完整;第2组:用Prophy Jet去除玷污层;第3组:用10%磷酸处理20秒;第4组:包括因牙冠中部横向骨折而暴露的牙本质。牙本质表面先用全粘结剂2及其配套粘结剂处理,然后用P50树脂复合材料,以1毫米的增量进行聚合。在37℃水中储存24小时后,以5毫米/分钟的十字头速度在剪切模式下对组件进行破坏测试。使用扫描电子显微镜对表面和界面形态进行表征。以兆帕为单位的值为:第1组:10.24±2.98;第2组:20.37±4.62;第3组:32.68±7.12;第4组:26.77±4.85。方差分析和学生t检验表明均值具有统计学差异(P<0.05)。由于仅在第4组的牙本质小管中以及第3组的小管和管间区域发现了明显的树脂渗透,因此得出结论,树脂渗透可为此全酸蚀系统的剪切粘结强度贡献约三分之一。