Chiral resolution of the dansyl derivative of 2-methyltaurine by capillary electrophoresis.
作者信息
Anselmi S, Braghiroli D, Di Bella M, Schmid M G, Wintersteiger R, Gübitz G
机构信息
Dipartimento di Scienze Farmaceutiche, Università di Modena, Italy.
出版信息
J Chromatogr B Biomed Appl. 1996 May 31;681(1):83-6. doi: 10.1016/0378-4347(95)00532-3.
PMID:8798916
Abstract
A cyclodextrin-modified micellar capillary electrophoretic method was developed for the chiral separation of 2-methyltaurine. The racemic mixture was separated after derivatization with dansyl chloride. The enantiomeric separation of the dansyl derivative was done using electrolyte solutions containing beta-cyclodextrin (beta-CD) or different ratios of beta- and gamma-CD. The mixture of beta- and gamma-CD optimally resolved the compound studied.
摘要
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