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食用油脂中的芥酸:采用开管(毛细管)气液色谱法测定的协作研究。

Erucic acid in edible fats and oils: a collaborative study on determination by open-tubular (capillary) gas-liquid chromatography.

作者信息

Ackman R G, Barlow S M, Duthie I F

出版信息

J Chromatogr Sci. 1977 Aug;15(8):290-5. doi: 10.1093/chromsci/15.8.290.

Abstract

An open-tubular (capillary) column gas-liquid chromatographic method for the determination of the specific isomer of docosenoic acid known as erucic acid (cis-docos-13-enoic) in the presence of other docosenoic acid isomers present in partially hydrogenated marine oils has been evaluated collaboratively. With wall-coated columns and the liquid phase SILAR-5CP, nine laboratories successfully analysed mixtures of partially hydrogenated marine oils, corn oil and rapeseed oil with a nominal content of 10% erucic acid, compatible with the regulations of the European Economic Community.

摘要

已协同评估了一种开管(毛细管)柱气液色谱法,用于在部分氢化海产油中存在的其他二十二碳烯酸异构体的情况下,测定被称为芥酸(顺式二十二碳 -13- 烯酸)的二十二碳烯酸特定异构体。使用涂壁柱和液相SILAR-5CP,九个实验室成功分析了标称芥酸含量为10%的部分氢化海产油、玉米油和菜籽油的混合物,符合欧洲经济共同体的规定。

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