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使用金钯合金对焊点和焊缝进行机械和元素特性分析。

Mechanical and elemental characterization of solder joints and welds using a gold-palladium alloy.

作者信息

Wiskott H W, Macheret F, Bussy F, Belser U C

机构信息

Division of Fixed Prosthodontics, University of Geneva, Switzerland.

出版信息

J Prosthet Dent. 1997 Jun;77(6):607-16. doi: 10.1016/s0022-3913(97)70103-3.

DOI:10.1016/s0022-3913(97)70103-3
PMID:9185054
Abstract

PURPOSE

This study was conducted to determine whether newer infrared or laser welding technologies created joints superior to traditional furnace or torch soldering methods of joining metals. It was designed to assess the mechanical resistance, the characteristics of the fractured surfaces, and the elemental diffusion of joints obtained by four different techniques: (1) preceramic soldering with a propane-oxygen torch, (2) postceramic soldering with a porcelain furnace, (3) preceramic and (4) postceramic soldering with an infrared heat source, and (5) laser welding.

MATERIAL AND METHODS

Mechanical resistance was determined by measuring the ultimate tensile strength of the joint and by determining their resistance to fatigue loading. Elemental diffusion to and from the joint was assessed with microprobe tracings. Scanning electron microscopy micrographs of the fractured surface were also obtained and evaluated.

RESULTS

Under monotonic tensile stress, three groups emerged: The laser welds were the strongest, the preceramic joints ranged second, and the postceramic joints were the weakest. Under fatigue stress, the order was as follows: first, the preceramic joints, and second, a group that comprised both postceramic joints and the laser welds. Inspection of the fractographs revealed several fracture modes but no consistent pattern emerged. Microprobe analyses demonstrated minor diffusion processes in the preceramic joints, whereas significant diffusion was observed in the postceramic joints.

CLINICAL IMPLICATIONS

The mechanical resistance data conflicted as to the strength that could be expected of laser welded joints. On the basis of fatigue resistance of the joints, neither infrared solder joints nor laser welds were stronger than torch or furnace soldered joints.

摘要

目的

本研究旨在确定更新的红外或激光焊接技术所形成的接头是否优于传统的炉中钎焊或火焰钎焊连接金属的方法。其设计目的是评估通过四种不同技术获得的接头的机械阻力、断裂表面特征以及元素扩散情况:(1)用丙烷 - 氧气火焰进行陶瓷前钎焊,(2)用烤瓷炉进行陶瓷后钎焊,(3)用红外热源进行陶瓷前钎焊,(4)用红外热源进行陶瓷后钎焊,以及(5)激光焊接。

材料与方法

通过测量接头的极限拉伸强度并确定其对疲劳载荷的抵抗力来测定机械阻力。用微探针追踪评估接头处元素的进出扩散情况。还获取并评估了断裂表面的扫描电子显微镜照片。

结果

在单调拉伸应力下,出现了三组情况:激光焊接接头最强,陶瓷前接头次之,陶瓷后接头最弱。在疲劳应力下,顺序如下:首先是陶瓷前接头,其次是包括陶瓷后接头和激光焊接接头的一组。对接头断口照片的检查揭示了几种断裂模式,但没有出现一致的模式。微探针分析表明陶瓷前接头中有轻微的扩散过程,而在陶瓷后接头中观察到明显的扩散。

临床意义

关于激光焊接接头预期强度的机械阻力数据存在冲突。基于接头的抗疲劳性,红外钎焊接头和激光焊接接头都不比火焰钎焊或炉中钎焊接头更强。

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