Xu Y J, Xie S X, Zhao H F, Han D, Xu T H, Xu D M
Academy of Traditional Chinese Medicine and Materia Medica of Jilin Province, Changchun 130021, China.
Yao Xue Xue Bao. 2001 Oct;36(10):750-3.
To investigate the chemical constituents of the fruit of Tribulus terrestris J..
Various chromatographic techniques were used to separate the chemical constituents. ESIMS, IR, 1HNMR, 13CNMR and HMBC were used to determine the structures of the isolated constituents.
Two new compounds were isolated from the fruits of Tribulus terrestris J. and were identified as neohecogenin-3-O-beta-D-glucopyranosyl (1-->2)-beta-D-glucopyranosyl (1-->4)-beta-D-galactopyranoside (I); neohecogenin-3-O-beta-D-glucopyranosyl (1-->4)-beta-D-galactopyranoside (II).
Compounds I and II are new steroidal saponins.
研究刺蒺藜果实的化学成分。
采用多种色谱技术分离化学成分。利用电喷雾离子化质谱(ESIMS)、红外光谱(IR)、核磁共振氢谱(1HNMR)、核磁共振碳谱(13CNMR)和异核多键相关谱(HMBC)确定分离得到的成分的结构。
从刺蒺藜果实中分离得到两个新化合物,分别鉴定为新海柯皂苷元-3-O-β-D-吡喃葡萄糖基(1→2)-β-D-吡喃葡萄糖基(1→4)-β-D-吡喃半乳糖苷(I);新海柯皂苷元-3-O-β-D-吡喃葡萄糖基(1→4)-β-D-吡喃半乳糖苷(II)。
化合物I和II是新的甾体皂苷。