Asmussen Erik, Peutzfeldt Anne
Department of Dental Materials, School of Dentistry, Faculty of Health Sciences, University of Copenhagen, Copenhagen, Denmark.
Eur J Oral Sci. 2005 Oct;113(5):417-21. doi: 10.1111/j.1600-0722.2005.00239.x.
This study measured the polymerization contraction of a resin composite cured at three levels of energy density, each attained at six different levels of power density. The polymerization contraction of the composite was recorded by the method of the deflecting disc (n = 5) for 1 h following the start of irradiation. Power densities of 50, 100, 200, 400, 800 and 1,000 mW cm(-2), as measured on a dental radiometer, were obtained by variation of distance and supply voltage of a commercial light-curing unit. The spectral distribution at each power density was recorded using a spectrophotometer. The absorption spectrum of camphorquinone was also recorded, and the efficiency of the radiation at each power density was calculated as the integral over wavelength of the product of absorption and emission. From the slope of the contraction curves, an approximation to the initial rate of polymerization, Rp, was calculated and was taken as an alternative measure of power density. Statistical analyses showed that polymerization contraction increased significantly with increasing levels of energy density received by the resin composite, and, for each level of energy density, that the contraction decreased significantly with increasing power density.
本研究测量了在三种能量密度水平下固化的树脂复合材料的聚合收缩,每种能量密度水平通过六种不同的功率密度水平获得。在开始照射后的1小时内,通过偏转盘法(n = 5)记录复合材料的聚合收缩。通过改变商用光固化单元的距离和电源电压,在牙科辐射计上测得的功率密度为50、100、200、400、800和1000 mW cm(-2)。使用分光光度计记录每种功率密度下的光谱分布。还记录了樟脑醌的吸收光谱,并将每种功率密度下的辐射效率计算为吸收和发射乘积在波长上的积分。根据收缩曲线的斜率,计算出聚合初始速率Rp的近似值,并将其作为功率密度的替代度量。统计分析表明,树脂复合材料接受的能量密度水平增加时,聚合收缩显著增加,并且对于每种能量密度水平,收缩随着功率密度的增加而显著降低。