[香鳞毛蕨萜类成分的研究]
[Study on terpene of Dryopteris fragrans L].
作者信息
Shen Zhi-Bin, Luo Wen-Ying, Yan You-Shao, Zhu Jun-Fang
机构信息
Guangdong University of Pharmacy, Guangzhou 510224, China.
出版信息
Zhong Yao Cai. 2006 Apr;29(4):334-5.
OBJECTIVE
To study the terpene of Dryopteris fragrans.
METHODS
Isolation and purification were carried out on repeated silica gel, Sephadex LH-20 column chromatography and prepare HPLC. The structures of the compounds were determined by physicochemical properties and spectral analysis.
RESULTS
Four compounds were isolated and identified as 10-hydroxyl-15-oxo-alpha-cadinol (I), albicany acetate (II), alpha-cadinene (III), albicanol (IV).
CONCLUSION
Compounds I is isolated from this plant for the first time.
目的
研究香鳞毛蕨的萜类成分。
方法
采用反复硅胶柱色谱、葡聚糖凝胶LH - 20柱色谱及制备型高效液相色谱进行分离纯化，通过理化性质和光谱分析确定化合物结构。
结果
分离鉴定了4个化合物，分别为10 - 羟基 - 15 - 氧代 - α - 杜松醇（I）、白檀醇乙酸酯（II）、α - 杜松烯（III）、白檀醇（IV）。
结论
化合物I首次从该植物中分离得到。
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