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填料分布对实验性树脂复合材料颜色参数的影响。

Influence of filler distribution on the color parameters of experimental resin composites.

作者信息

Lim Yong-Kyu, Lee Yong-Keun, Lim Bum-Soon, Rhee Sang-Hoon, Yang Hyeong-Cheol

机构信息

Department of Orthodontics, Graduate School of Clinical Dentistry, Korea University, Seoul, Republic of Korea.

出版信息

Dent Mater. 2008 Jan;24(1):67-73. doi: 10.1016/j.dental.2007.02.007. Epub 2007 Apr 8.

Abstract

OBJECTIVES

Simulating the optical properties of natural tooth would be the final goal for esthetic restorative materials. Filler distribution in resin composites determines the scattering in composite materials, which in turn would influence the color parameters such as lightness, chroma and hue. The objective of this study was to determine the influence of filler size and amount on the color parameters of experimental resin composites.

METHOD

Color of 11 experimental resin composites with two different sized fillers (LG: 0.77 microm and SG: 0.50 microm) in 10-70 wt% was measured by a spectrophotometer. Color coordinates (CIE L*, a* and b*), chroma and hue angle were determined. Optical constants including scattering coefficient (S), absorption coefficient (K) and light reflectivity (RI) were calculated. To determine the influence of the amount of filler on the optical parameters, Pearson correlations between the amount of filler (%) and color parameters and optical constants were calculated. Correlations between the optical constants (S, K and RI) and color parameters were calculated (p<0.05).

RESULTS

S value increased as the amount of filler increased. RI value generally increased as the amount of filler increased for LG filler group, and increased up to 40% filler for SG filler group. CIE L* value increased as the amount of filler increased in both of LG and SG filler groups. CIE L* value was highly correlated with S and RI values for both filler groups (r=0.961-0.974).

CONCLUSION

Lightness was highly correlated with the amount of filler, S and RI values (r=0.932-0.974). But the correlation coefficients between the amount of filler and chroma/hue were moderate (r=0.406-0.827); therefore, pigmentation would be tried to simulate the color of resin composites to those of natural tooth. Optical properties of resin composites could be partly simulated to those of teeth by controlling the filler distribution.

摘要

目的

模拟天然牙齿的光学特性是美学修复材料的最终目标。树脂复合材料中的填料分布决定了复合材料中的散射,进而会影响诸如明度、彩度和色调等颜色参数。本研究的目的是确定填料尺寸和含量对实验性树脂复合材料颜色参数的影响。

方法

用分光光度计测量11种实验性树脂复合材料的颜色,这些复合材料含有两种不同尺寸的填料(LG:0.77微米和SG:0.50微米),填料含量为10%-70%重量比。确定颜色坐标(CIE L*、a和b)、彩度和色调角。计算包括散射系数(S)、吸收系数(K)和光反射率(RI)在内的光学常数。为了确定填料含量对光学参数的影响,计算填料含量(%)与颜色参数和光学常数之间的皮尔逊相关性。计算光学常数(S、K和RI)与颜色参数之间的相关性(p<0.05)。

结果

随着填料含量的增加,S值增加。对于LG填料组,RI值通常随着填料含量的增加而增加,对于SG填料组,填料含量增加到40%时RI值增加。在LG和SG填料组中,CIE L值均随着填料含量的增加而增加。对于两个填料组,CIE L值与S和RI值高度相关(r=0.961-0.974)。

结论

明度与填料含量、S和RI值高度相关(r=0.932-0.974)。但填料含量与彩度/色调之间的相关系数为中等(r=0.406-0.827);因此,将尝试通过色素沉着使树脂复合材料的颜色模拟天然牙齿的颜色。通过控制填料分布,树脂复合材料的光学特性可以部分模拟牙齿的光学特性。

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