通过分子内Heck还原环化高效合成3-苯并氮杂卓骨架。
Efficient synthesis of the 3-benzazepine framework via intramolecular Heck reductive cyclization.
作者信息
Donets Pavel A, Van der Eycken Erik V
机构信息
Laboratory for Organic & Microwave-Assisted Chemistry (LOMAC), Department of Chemistry, University of Leuven, Celestijnenlaan 200F, B-3001 Leuven, Belgium.
出版信息
Org Lett. 2007 Aug 2;9(16):3017-20. doi: 10.1021/ol071079g. Epub 2007 Jul 3.
PMID:17608431
Abstract
A microwave-assisted protocol based on reductive Heck reaction was developed for regio- and stereoselective construction of the 3-benzazepine core.
摘要
基于还原Heck反应开发了一种微波辅助方案，用于区域和立体选择性构建3-苯并氮杂卓核心。
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