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采用多种技术手段研究两种不同抛光处理后三种纳米复合材料的表面粗糙度和形貌。

Surface roughness and morphology of three nanocomposites after two different polishing treatments by a multitechnique approach.

机构信息

University of Strasbourg, France.

出版信息

Dent Mater. 2010 May;26(5):416-25. doi: 10.1016/j.dental.2009.09.014. Epub 2010 Jan 25.

Abstract

OBJECTIVES

The purpose of this study was to assess the surface roughness and morphology of three nanocomposites polished with two different polishing systems.

METHODS

Specimens made of hybrid composite (Tetric Ceram [TC] as control) and nanocomposites: nanofilled (Filtek Supreme [FS]), nanofilled hybrid (Grandio [Gr]), complex nanofilled hybrid (Synergy D6 [Syn]) were polished with CompoSystem [CS] or Sof-Lex [SL] polishing discs. The average surface roughness (Ra) before and after polishing was measured using optical profilometry. Both AFM and SEM techniques were additionally used to analyze the surface morphology after polishing with the aim of relating the surface morphology and the surface roughness. Statistical analysis was done by ANOVA using a general linear model (alpha=0.05) with an adjustment for multiple comparisons.

RESULTS

Within the same polishing system, FS exhibited the smoothest surface, followed by Syn, TC and Gr (p<0.0001). Sof-Lex polishing discs produced the smoothest surface compared to CompoSystem (p<0.0001). AFM and SEM observations confirmed that the surface roughness was related to the surface morphology and to the average filler size.

SIGNIFICANCE

Positive correlation between the average filler size and the surface roughness suggest that using nanoparticles in the formulation does not necessary improve the surface texture. The nanofilled composite FS, which contains only nanofillers, showed the best results when associated to Sof-Lex polishing discs.

摘要

目的

本研究旨在评估三种纳米复合材料经两种不同抛光系统抛光后的表面粗糙度和形貌。

方法

采用混合复合材料(Tetric Ceram [TC] 作为对照)和纳米复合材料:纳米填充型(Filtek Supreme [FS])、纳米混合填充型(Grandio [Gr])、复合纳米混合填充型(Synergy D6 [Syn])制作试件,用 CompoSystem [CS] 或 Sof-Lex [SL] 抛光片进行抛光。采用光学轮廓仪测量抛光前后的平均表面粗糙度(Ra)。此外,还使用 AFM 和 SEM 技术分析抛光后的表面形貌,旨在将表面形貌与表面粗糙度联系起来。采用一般线性模型(alpha=0.05)进行方差分析,并进行多次比较调整。

结果

在相同的抛光系统中,FS 表现出最光滑的表面,其次是 Syn、TC 和 Gr(p<0.0001)。与 CompoSystem 相比,Sof-Lex 抛光片产生的表面更光滑(p<0.0001)。AFM 和 SEM 观察结果证实,表面粗糙度与表面形貌和平均填料尺寸有关。

意义

平均填料尺寸与表面粗糙度之间的正相关表明,在配方中使用纳米颗粒不一定能改善表面纹理。含有仅纳米填料的纳米填充型复合材料 FS,与 Sof-Lex 抛光片联合使用时效果最佳。

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