Department of Chemistry, College of Education, University of Basrah, Iraq.
Molecules. 2010 Nov 17;15(11):8425-30. doi: 10.3390/molecules15118425.
Novel 2,3-dihydro-4-pyridinones were synthesized via the reaction of curcumin and primary amines or amine acetates under microwave irradiation. Montmorillonite K-10 was used as a catalyst. Reaction times did not exceed 120 s. The structures of the compounds were established by elemental analysis and from their mass, 1H- and 13C-NMR spectra.
新型 2,3-二氢-4-吡啶酮通过姜黄素与伯胺或胺乙酸盐在微波辐射下的反应合成。蒙脱土 K-10 用作催化剂。反应时间不超过 120 秒。通过元素分析和它们的质谱、1H-NMR 和 13C-NMR 谱确定了化合物的结构。