（E）-N'-（3,5-二溴-2-羟基-亚苄基）-2-甲氧基-苯甲酰肼
(E)-N'-(3,5-Dibromo-2-hydroxy-benzyl-idene)-2-methoxy-benzohydrazide.
作者信息
Cao Guo-Biao, Lu Xu-Hui
机构信息
Department of Chemistry, Ankang University, Ankang Shanxi 725000, People's Republic of China.
出版信息
Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 17;65(Pt 7):o1587. doi: 10.1107/S1600536809022168.
The title compound, C(15)H(12)Br(2)N(2)O(3), was synthesized by the reaction of 3,5-dibromo-2-hydroxy-benzaldehyde with an equimolar quantity of 2-methoxy-benzohydrazide in methanol. The dihedral angle between the two benzene rings is 3.4 (2)° and intra-molecular O-H⋯N and N-H⋯O hydrogen bonds are observed in the mol-ecule. The crystal studied was an inversion twin with a 0.513 (19):0.487 (19) domain ratio.
标题化合物C(15)H(12)Br(2)N(2)O(3)是通过3,5-二溴-2-羟基苯甲醛与等摩尔量的2-甲氧基苯甲酰肼在甲醇中反应合成的。两个苯环之间的二面角为3.4 (2)°，并且在分子中观察到分子内O-H⋯N和N-H⋯O氢键。所研究的晶体是一个倒易孪晶，畴比为0.513 (19):0.487 (19)。
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