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(E)-N'-(3,5-Dibromo-2-hydroxy-benzyl-idene)-2-methoxy-benzohydrazide.

作者信息

Cao Guo-Biao, Lu Xu-Hui

机构信息

Department of Chemistry, Ankang University, Ankang Shanxi 725000, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 17;65(Pt 7):o1587. doi: 10.1107/S1600536809022168.

Abstract

The title compound, C(15)H(12)Br(2)N(2)O(3), was synthesized by the reaction of 3,5-dibromo-2-hydroxy-benzaldehyde with an equimolar quantity of 2-methoxy-benzohydrazide in methanol. The dihedral angle between the two benzene rings is 3.4 (2)° and intra-molecular O-H⋯N and N-H⋯O hydrogen bonds are observed in the mol-ecule. The crystal studied was an inversion twin with a 0.513 (19):0.487 (19) domain ratio.

摘要
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/0f68/2969285/96197724456e/e-65-o1587-fig1.jpg

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