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N'-(5-溴-2-甲氧基-亚苄基)-2-甲氧基-苯甲酰肼

N'-(5-Bromo-2-methoxy-benzyl-idene)-2-methoxy-benzohydrazide.

作者信息

Lin Xue-Song, Sang Ya-Li

机构信息

Department of Chemistry, Chifeng University, Chifeng 024001, People's Republic of China.

出版信息

Acta Crystallogr Sect E Struct Rep Online. 2009 Jun 20;65(Pt 7):o1649. doi: 10.1107/S1600536809022971.

DOI:10.1107/S1600536809022971
PMID:21582913
原文链接:https://pmc.ncbi.nlm.nih.gov/articles/PMC2969363/
Abstract

The title hydrazone compound, C(16)H(15)BrN(2)O(3), adopts an E configuration about the C=N double bond. The mol-ecule is twisted, the dihedral angle between the two substituted benzene rings being 22.0 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O hydrogen bonds, forming chains along the c axis.

摘要

腙化合物C(16)H(15)BrN(2)O(3)围绕C=N双键采取E构型。分子呈扭曲状，两个取代苯环之间的二面角为22.0 (2)°。在晶体结构中，分子通过分子间N-H⋯O氢键相连，沿c轴形成链状结构。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c673/2969363/6af09b5ebab3/e-65-o1649-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c673/2969363/250ba03ec4c0/e-65-o1649-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c673/2969363/6af09b5ebab3/e-65-o1649-fig2.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c673/2969363/250ba03ec4c0/e-65-o1649-fig1.jpg
https://cdn.ncbi.nlm.nih.gov/pmc/blobs/c673/2969363/6af09b5ebab3/e-65-o1649-fig2.jpg

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本文引用的文献

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Acta Crystallogr Sect E Struct Rep Online. 2009 Mar 6;65(Pt 4):o688. doi: 10.1107/S1600536809007466.
2
3,4,5-Trihydr-oxy-N'-(1H-indol-3-yl-methyl-idene)benzohydrazide penta-hydrate.3,4,5-三羟基-N'-(1H-吲哚-3-基亚甲基)苯甲酰肼五水合物
Acta Crystallogr Sect E Struct Rep Online. 2008 Nov 29;64(Pt 12):o2481. doi: 10.1107/S1600536808039342.
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