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[气相色谱-质谱联用仪对黄精及其炮制品挥发性成分的比较分析]

[Comparative analysis of volatile fractions in Polygonati rhizoma and its processed products by GC-MS].

作者信息

Wang Jin, Yue Yongde, Tang Feng, Tao Wuqun

机构信息

Key Laboratory of Bamboo and Rattan Science and Technology of State Forestry Administration, International Center for Bamboo and Rattan, Beijing 100102, China.

出版信息

Zhongguo Zhong Yao Za Zhi. 2011 Aug;36(16):2187-91.

PMID:22097326
Abstract

OBJECTIVE

To conduct comparative study on the volatile components from Polygonati Rhizoma during processing.

METHOD

Volatile oil was obtained from Polygonati Rhizoma by steam distillation (SD). Volatile components were concentrated by a purge and trap-thermal desorption (P&T-TD) method, and analyzed with gas chromatography-mass spectrometry (GC-MS), which were comparative by analyzed with the method of SD-GC-MS simultaneously.

RESULT

The change in quantity and quality of volatile components in pre and post processed Polygonati Rhizoma were observed. Fifty-one compounds were checked out with SD-GC-MS, while 11 compounds with P&T-TD-GC-MS.

CONCLUSION

This study is useful to illustrate the mechanism of decreasing toxicity and stimulating components after being processed.

摘要

目的

对黄精炮制前后的挥发性成分进行对比研究。

方法

采用水蒸气蒸馏法(SD)从黄精中提取挥发油。通过吹扫捕集-热脱附(P&T-TD)法浓缩挥发性成分,并用气相色谱-质谱联用仪(GC-MS)进行分析,同时与SD-GC-MS法进行对比分析。

结果

观察到黄精炮制前后挥发性成分在数量和质量上的变化。SD-GC-MS法检出51种化合物,而P&T-TD-GC-MS法检出11种化合物。

结论

本研究有助于阐明黄精炮制后减毒及刺激性成分降低的机制。

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