Phytochemical Research Laboratory, Department of Industrial Pharmacy, Federal University of Santa Maria, Build 26, Room 1115, Santa Maria, RS 97105-900, Brazil.
Nat Prod Res. 2013;27(1):68-71. doi: 10.1080/14786419.2011.653971. Epub 2012 Jan 24.
The essential oils obtained by hydrodistillation from the leaves of Tabernaemontana catharinensis had their composition analysed by GC-MS. A total of 18 substances were identified, consisting of a complex mixture of sesquiterpenes (83.52%), monoterpenes (5.46%) and triterpenes (4.56%). The main components in the oil were β-caryophyllene (56.87%), α-cadinol (12.52%), 8S,13-cedran-diol (5.41%), α-terpineol (3.99%), β-eudesmol (2.54%), caryophyllene oxide (2.51%) and ethyl iso-allocholate (2.03%) along with β-cubebene, γ-cadinene, cubenol, 1,8-cineol, o-cymene, curcumenol, spathulenol, friedeline and β-sitosterol as minor constituents. An antioxidant property was tested with the oil obtained by means of 1,1-diphenyl-2-picrylhydrazyl assay; the oil presented interesting radical scavenging activity. To the best of our knowledge, this is the first study of the composition and antioxidant activity of essential oil from the T. catharinensis collected from Brazil.
采用水蒸馏法从三叶苦荬菜的叶子中提取的精油,通过 GC-MS 对其成分进行了分析。共鉴定出 18 种物质,主要由倍半萜烯(83.52%)、单萜烯(5.46%)和三萜烯(4.56%)组成。该油的主要成分是β-石竹烯(56.87%)、α-杜松醇(12.52%)、8S,13-雪松二醇(5.41%)、α-松油醇(3.99%)、β-桉叶油醇(2.54%)、石竹烯氧化物(2.51%)和异乙基鹅去氧胆酸(2.03%),以及β-古巴烯、γ-杜松烯、古巴醇、1,8-桉树脑、对伞花烃、莪术醇、斯巴醇、friedeline 和β-谷甾醇等少量成分。采用 1,1-二苯基-2-苦基肼法对所得到的精油进行了抗氧化性能测试;该油表现出了有趣的自由基清除活性。据我们所知,这是首次对从巴西三叶苦荬菜中提取的精油的成分和抗氧化活性进行研究。