Jamshidvand Arezoo, Kia Reza, Kargar Hadi, Tahir Muhammad Nawaz
Acta Crystallogr Sect E Struct Rep Online. 2012 Feb 1;68(Pt 2):o292. doi: 10.1107/S1600536811055905. Epub 2012 Jan 7.
The asymmetric unit of the title compound, C(30)H(28)N(2)O(2), comprises half of a potential tetra-dentate Schiff base ligand; an inversion centre is situtated at the center of the butane-diamine spacer. The central methyl-ene segment of the diamine spacer is disordered over two positions with a refined site-occupancy ratio of 0.651 (7):0.349 (7). The phenyl ring and the hy-droxy-substituted benzene ring are almost perpendicular to each other, with a dihedral angle of 87.90 (8) Å. Intra-molecular O-H⋯N hydrogen bonds make S(6) ring motifs.
标题化合物C(30)H(28)N(2)O(2)的不对称单元包含一个潜在四齿席夫碱配体的一半;一个倒转中心位于丁二胺间隔基的中心。二胺间隔基的中心亚甲基片段在两个位置上无序,精修的位点占有率比为0.651 (7):0.349 (7)。苯环和羟基取代的苯环几乎相互垂直,二面角为87.90 (8) Å。分子内O-H⋯N氢键形成S(6)环模式。