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驱动振幅调制原子力显微镜:从真空到液体。

Drive-amplitude-modulation atomic force microscopy: From vacuum to liquids.

机构信息

Departamento de Física de la Materia Condensada, Universidad Autónoma de Madrid, E-28049 Madrid, Spain.

出版信息

Beilstein J Nanotechnol. 2012;3:336-44. doi: 10.3762/bjnano.3.38. Epub 2012 Apr 18.

Abstract

We introduce drive-amplitude-modulation atomic force microscopy as a dynamic mode with outstanding performance in all environments from vacuum to liquids. As with frequency modulation, the new mode follows a feedback scheme with two nested loops: The first keeps the cantilever oscillation amplitude constant by regulating the driving force, and the second uses the driving force as the feedback variable for topography. Additionally, a phase-locked loop can be used as a parallel feedback allowing separation of the conservative and nonconservative interactions. We describe the basis of this mode and present some examples of its performance in three different environments. Drive-amplutide modulation is a very stable, intuitive and easy to use mode that is free of the feedback instability associated with the noncontact-to-contact transition that occurs in the frequency-modulation mode.

摘要

我们介绍了驱动幅度调制原子力显微镜作为一种动态模式,在从真空到液体的所有环境中都具有出色的性能。与频率调制一样,新的模式采用具有两个嵌套环的反馈方案:第一个环通过调节驱动力使悬臂的振动幅度保持恒定,第二个环使用驱动力作为反馈变量来测量形貌。此外,还可以使用锁相环作为并行反馈,从而分离保守和非保守相互作用。我们描述了这种模式的基础,并展示了它在三种不同环境中的一些性能示例。驱动幅度调制是一种非常稳定、直观和易于使用的模式,它没有与频率调制模式中发生的非接触到接触过渡相关的反馈不稳定性。

https://cdn.ncbi.nlm.nih.gov/pmc/blobs/fcac/3343270/c3ccc4777e6d/Beilstein_J_Nanotechnol-03-336-g002.jpg

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