Modi Mohammed H, Rai S K, Idir Mourad, Schaefers F, Lodha G S
X-ray Optics Section, Raja Ramanna Centre for Advanced Technology Indore 452013, India.
Opt Express. 2012 Jul 2;20(14):15114-20. doi: 10.1364/OE.20.015114.
In the present study we report a new multilayer combination comprised of refracting layers of niobium carbide and spacer layers of silicon as a more stable and high reflecting combination for the 10 - 20 nm wavelength region. The reflectivity of the new combination is comparable to Mo/Si conventional mirrors. Annealing experiments carried out with NbC/Si multilayer at 600°C temperature showed a ~2.5% drop in the soft x-ray reflectivity along with a marginal contraction in the multilayer period length. The multilayer structure is found stable after the heat treatment. Crystallization of the niobium carbide and silicon layers is responsible for the compaction in the period length as revealed by the grazing incidence x-ray diffraction measurements. No signature of silicide formation or any other chemical species could be detected. The multilayer structures were grown by ion beam sputtering technique using a compound target of niobium carbide. Soft x-ray reflectivity measurements performed at the Indus-1 and BESSY-II synchrotron radiation sources are found in good agreement with the simulations.
在本研究中,我们报道了一种新的多层组合,它由碳化铌折射层和硅间隔层组成,是一种在10 - 20纳米波长区域更稳定且高反射的组合。这种新组合的反射率与传统的Mo/Si镜子相当。在600°C温度下对NbC/Si多层膜进行的退火实验表明,软X射线反射率下降了约2.5%,同时多层膜周期长度略有收缩。热处理后发现多层结构是稳定的。掠入射X射线衍射测量表明,碳化铌层和硅层的结晶是周期长度压缩的原因。未检测到硅化物形成或任何其他化学物种的迹象。多层结构是使用碳化铌复合靶通过离子束溅射技术生长的。在Indus-1和BESSY-II同步辐射源进行的软X射线反射率测量结果与模拟结果吻合良好。