Heilongjiang Academy of TCM, Heilongjiang University of Chinese Medicine, Harbin 150040, China.
Molecules. 2012 Oct 26;17(11):12651-6. doi: 10.3390/molecules171112651.
To study the chemical constituents of the fruits of noni (Morinda citrifolia L.), and find novel compounds, an n-butanol extract of the ethanol soluble fraction was subjected to repeated silica gel and ODS column chromatography and HPLC. Two new glycosides were isolated and their structures elucidated by NMR and HRFAB-MS spectrometry as (2E,4E,7Z)-deca-2,4,7-trienoate-2-O-β-D-glucopyranosyl-β-D-glucopyranoside and amyl-1-O-β-D-apio-furanosyl-1,6-O-β-D-glucopyranoside, respectively.
为了研究诺丽果（Morinda citrifolia L.）的化学成分，寻找新的化合物，对乙醇可溶部分的正丁醇提取物进行了反复的硅胶和 ODS 柱层析和 HPLC 分离。分离得到了两个新的糖苷，并通过 NMR 和 HRFAB-MS 光谱确定了它们的结构，分别为（2E,4E,7Z）-癸-2,4,7-三烯酸-2-O-β-D-吡喃葡萄糖基-β-D-吡喃葡萄糖苷和淀粉-1-O-β-D-阿洛呋喃基-1,6-O-β-D-吡喃葡萄糖苷。
