Department of Chemical Engineering and Environmental Technology, Faculty of Chemistry, University of Oviedo, Julián Clavería 8, 33006 Oviedo, Spain.
Bioresour Technol. 2013 Jul;139:1-4. doi: 10.1016/j.biortech.2013.03.197. Epub 2013 Apr 12.
This work proposes a 25 min-last thermogravimetric method as a tool to determine biomass sample's proximate analysis data (moisture, ash, volatile matter and fixed carbon contents) just by direct measure of weight changes on each sample's TG chart. Compared with international standards commonly used to that aim, TG is a faster and easier to develop technique. Obtained results were satisfactory, with AEE under 6% for moisture and volatile matter, close to 10% for fixed carbon determination and AAD of 1.6 points for ash content.
本工作提出了一种 25 分钟的热重法,作为一种通过直接测量每个样品的 TG 图谱上的重量变化来确定生物质样品的近似分析数据(水分、灰分、挥发分和固定碳含量)的工具。与通常用于该目的的国际标准相比,TG 是一种更快、更容易开发的技术。得到的结果令人满意,水分和挥发分的 AEE 低于 6%,固定碳的测定接近 10%,灰分的 AAD 为 1.6 点。