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采用火焰原子吸收光谱法评价土耳其家用洗涤剂样品中的金属含量。

Evaluation of metal contents of household detergent samples from Turkey by flame atomic absorption spectrometry.

机构信息

Faculty of Science, Chemistry Department, Erciyes University, 38039, Kayseri, Turkey,

出版信息

Environ Monit Assess. 2013 Nov;185(11):9663-8. doi: 10.1007/s10661-013-3281-5. Epub 2013 May 31.

Abstract

The concentrations of cadmium, copper, chromium, cobalt, iron, lead, manganese, nickel, and zinc in detergent samples from Kayseri, Turkey were determined by flame atomic absorption spectrometry. HClO₄ (10 mL)/HNO₃ (10 mL) mixture was used for the digestion of household detergent samples. The correctness of the analytical procedures was checked with standard addition-recovery tests in different detergent samples for the investigated metal ions. The concentration ranges of the elements in the detergent samples were found as 17.2-60.1, 11.1-40.1, 2.5-32.3, 8.1-10.5, 7.2-21.6, 9.8-17.9, 1.7-3.8, 12.5-22.5, and 2.0-5.8 μg/g for iron, manganese, zinc, copper, lead, cobalt, cadmium, nickel, and chromium, respectively. The values found in this work were compared with some other studies around the world conducted on detergent samples.

摘要

采用火焰原子吸收光谱法测定了来自土耳其开塞利市的洗涤剂样品中镉、铜、铬、钴、铁、铅、锰、镍和锌的浓度。使用 HClO₄(10 毫升)/HNO₃(10 毫升)混合物对家用洗涤剂样品进行消解。通过在不同洗涤剂样品中进行标准添加回收测试,检查了分析程序的正确性。在所研究的金属离子中,洗涤剂样品中各元素的浓度范围分别为 17.2-60.1μg/g 铁、11.1-40.1μg/g 锰、2.5-32.3μg/g 锌、8.1-10.5μg/g 铜、7.2-21.6μg/g 铅、9.8-17.9μg/g 钴、1.7-3.8μg/g 镉、12.5-22.5μg/g 镍和 2.0-5.8μg/g 铬。本工作所得结果与世界各地对洗涤剂样品进行的一些其他研究进行了比较。

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