Wang Ping, Xu Jing, Wang Qi, Feng Shi-Xiu, Chen Tao, Zhang Cun-Li
College of Life Science, Northwest A&F University, Yangling 712100, China.
Zhongguo Zhong Yao Za Zhi. 2013 May;38(10):1531-5.
The chemical constituents were separated and purified from the roots and rhizomes of Smilax scobinicaulis by various chromatographic methods including silica gel, Sephadex LH-20. Their structures were obtained and identified as resveratrol-3-O-beta-D-glucopyranosyl-(1-->3)-beta-D-glucopyranoside (1), resveratrol (2), 8-viniferin (3), ethyl caffeate (4), 1-0-caffeoylglycerol (5), 1-O-p-coumaroylglycerol (6), 1-0-feruloylglycerol (7), grossamide (8), moracin M (9) on the analysis of spectroscopic data. Compound 1 was a new compound and compounds 3-5, 8,9 were separated from this plant for the first time.
采用硅胶、葡聚糖凝胶LH - 20等多种色谱方法从菝葜的根状茎中分离纯化化学成分。通过光谱数据分析确定其结构,分别为白藜芦醇 - 3 - O - β - D - 吡喃葡萄糖基 - (1→3) - β - D - 吡喃葡萄糖苷(1)、白藜芦醇(2)、8 - 葡萄素(3)、咖啡酸乙酯(4)、1 - O - 咖啡酰甘油(5)、1 - O - 对香豆酰甘油(6)、1 - O - 阿魏酰甘油(7)、粗糠酰胺(8)、桑辛素M(9)。化合物1为新化合物,化合物3 - 5、8、9为首次从该植物中分离得到。