Rodrigues I, Handl J, Binder E M
a BIOMIN Holding GmbH , Industriestrasse 21 , 3130 Herzogenburg , Austria.
Food Addit Contam Part B Surveill. 2011;4(3):168-79. doi: 10.1080/19393210.2011.589034. Epub 2011 Jul 12.
Between February and October 2009, 324 grain, feed and feed commodity samples were sourced directly at animal farms or feed production sites in Middle East and Africa and tested for the presence of A- and B-trichothecenes, zearalenone, fumonisins, aflatoxins and ochratoxin A, or for selected groups of mycotoxins only. Samples were analyzed after clean-up by immunoaffinity or solid-phase extraction followed by HPLC with derivatization where appropriate and fluorescence, UV or mass spectrometric detection. The percentage of positive samples of B-trichothecenes ranged from 0 to 87% of tested samples. The prevalence of fumonisins in the different countries was >50% in most cases. Zearalenone was present in tested commodities from all countries except three. The presence of aflatoxin in analyzed samples varied from 0 to 94%. Ochratoxin A was present in 67% of samples in Sudan and in 100% of Nigerian samples. No A-trichothecenes were found in this survey.
2009年2月至10月期间,直接从中东和非洲的养殖场或饲料生产场所采集了324份谷物、饲料及饲料商品样本,检测其中A、B型单端孢霉烯族毒素、玉米赤霉烯酮、伏马菌素、黄曲霉毒素和赭曲霉毒素A的存在情况,或仅检测部分霉菌毒素组。样本经免疫亲和或固相萃取净化后,在适当情况下进行衍生化处理,然后采用高效液相色谱法及荧光、紫外或质谱检测进行分析。B型单端孢霉烯族毒素阳性样本的比例在检测样本的0%至87%之间。在大多数情况下,不同国家伏马菌素的检出率均超过50%。除三个国家外,所有国家的检测商品中均存在玉米赤霉烯酮。分析样本中黄曲霉毒素的存在比例在0%至94%之间。苏丹67%的样本及尼日利亚100%的样本中存在赭曲霉毒素A。本次调查未发现A型单端孢霉烯族毒素。