Warwick Tony, Chuang Yi De, Voronov Dmitriy L, Padmore Howard A
Advanced Light Source, Lawrence Berkeley National Laboratory, Berkeley, CA 94720, USA.
J Synchrotron Radiat. 2014 Jul;21(Pt 4):736-43. doi: 10.1107/S1600577514009692. Epub 2014 Jun 3.
The optical design of a two-dimensional imaging soft X-ray spectrometer is described. A monochromator will produce a dispersed spectrum in a narrow vertical illuminated stripe (∼2 µm wide by ∼2 mm tall) on a sample. The spectrometer will use inelastically scattered X-rays to image the extended field on the sample in the incident photon energy direction (vertical), resolving the incident photon energy. At the same time it will image and disperse the scattered photons in the orthogonal (horizontal) direction, resolving the scattered photon energy. The principal challenge is to design a system that images from the flat-field illumination of the sample to the flat field of the detector and to achieve sufficiently high spectral resolution. This spectrometer provides a completely parallel resonant inelastic X-ray scattering measurement at high spectral resolution (∼30,000) over the energy bandwidth (∼5 eV) of a soft X-ray absorption resonance.
本文描述了一种二维成像软X射线光谱仪的光学设计。单色仪将在样品上的一条狭窄垂直照明条纹(约2微米宽,约2毫米高)中产生色散光谱。该光谱仪将使用非弹性散射X射线在入射光子能量方向(垂直方向)对样品上的扩展场进行成像,分辨入射光子能量。同时,它将在正交(水平)方向对散射光子进行成像和色散,分辨散射光子能量。主要挑战在于设计一个从样品的平面场照明到探测器平面场进行成像的系统,并实现足够高的光谱分辨率。该光谱仪在软X射线吸收共振的能量带宽(约5电子伏特)上,以高光谱分辨率(约30000)提供完全平行的共振非弹性X射线散射测量。