Morgan Andrew J, Prasciolu Mauro, Andrejczuk Andrzej, Krzywinski Jacek, Meents Alke, Pennicard David, Graafsma Heinz, Barty Anton, Bean Richard J, Barthelmess Miriam, Oberthuer Dominik, Yefanov Oleksandr, Aquila Andrew, Chapman Henry N, Bajt Saša
Center for Free-Electron Laser Science, DESY, Notkestrasse 85, 22607 Hamburg, Germany.
Photon Science, DESY, Notkestrasse 85, 22607 Hamburg, Germany.
Sci Rep. 2015 Jun 1;5:9892. doi: 10.1038/srep09892.
The ever-increasing brightness of synchrotron radiation sources demands improved X-ray optics to utilise their capability for imaging and probing biological cells, nanodevices, and functional matter on the nanometer scale with chemical sensitivity. Here we demonstrate focusing a hard X-ray beam to an 8 nm focus using a volume zone plate (also referred to as a wedged multilayer Laue lens). This lens was constructed using a new deposition technique that enabled the independent control of the angle and thickness of diffracting layers to microradian and nanometer precision, respectively. This ensured that the Bragg condition is satisfied at each point along the lens, leading to a high numerical aperture that is limited only by its extent. We developed a phase-shifting interferometric method based on ptychography to characterise the lens focus. The precision of the fabrication and characterisation demonstrated here provides the path to efficient X-ray optics for imaging at 1 nm resolution.
同步辐射源不断提高的亮度要求改进X射线光学器件,以便利用其在纳米尺度上对生物细胞、纳米器件和功能物质进行成像和探测的能力,并具备化学敏感性。在此,我们展示了使用体波带片(也称为楔形多层劳厄透镜)将硬X射线束聚焦到8纳米的焦点上。该透镜采用一种新的沉积技术构建,该技术能够分别将衍射层的角度和厚度独立控制到微弧度和纳米精度。这确保了沿透镜的每个点都满足布拉格条件,从而产生仅受其范围限制的高数值孔径。我们开发了一种基于叠层衍射成像的相移干涉测量方法来表征透镜焦点。此处展示的制造和表征精度为实现1纳米分辨率成像的高效X射线光学器件提供了途径。