Leclere Cédric, Cornelius Thomas W, Ren Zhe, Davydok Anton, Micha Jean-Sébastien, Robach Odile, Richter Gunther, Belliard Laurent, Thomas Olivier
Aix-Marseille Université, CNRS, Université de Toulon, IM2NP UMR 7334, 13397 Marseille, France.
CEA, INAC, SP2M/NRS, 17 rue des Martyrs, 38054 Grenoble, France.
J Appl Crystallogr. 2015 Jan 30;48(Pt 1):291-296. doi: 10.1107/S1600576715001107. eCollection 2015 Feb 1.
This article reports on the first successful combination of micro Laue (µLaue) diffraction with an atomic force microscope for nanomechanical tests of individual nanostructures. three-point bending on self-suspended gold nanowires was performed on the BM32 beamline at the ESRF using a specially designed atomic force microscope. During the bending process of the self-suspended wire, the evolution of µLaue diffraction patterns was monitored, allowing for extraction of the bending angle of the nanowire. This bending compares well with finite element analysis taking into account elastic constant bulk values and geometric nonlinearities. This novel experimental setup opens promising perspectives for studying mechanical properties at the nanoscale.
本文报道了首次成功将微劳厄(µLaue)衍射与原子力显微镜相结合,用于单个纳米结构的纳米力学测试。使用专门设计的原子力显微镜,在欧洲同步辐射装置(ESRF)的BM32光束线上对自支撑金纳米线进行了三点弯曲试验。在自支撑纳米线的弯曲过程中,监测了µLaue衍射图案的演变,从而能够提取纳米线的弯曲角度。这种弯曲与考虑弹性常数体值和几何非线性的有限元分析结果吻合良好。这种新颖的实验装置为研究纳米尺度的力学性能开辟了广阔的前景。