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气相色谱-质谱联用分析栀子及其炮制品中的挥发性成分

[Analysis of volatile ingredients in Gardeniae Fructus and its processed products by GC-MS].

作者信息

Liu Hui, Yao Lan, Chen Jian-hong, Gu Xue-zhu, Ma Yin-lian, Chen Ying, Li Pu-ling, Zhang Cun

出版信息

Zhongguo Zhong Yao Za Zhi. 2015 May;40(9):1732-7.

Abstract

Gardeniae Fructus contains volatile ingredients, however, the species and proportions in different processed products of Gardeniae Fructus are different. In this experiment, volatile ingredients were separated by steam distillation with content of 1.2, 1.0, 0.9, 0.7 µL · g(-1) in Gardeniae Fructus, fried Gardeniae Fructus, stir-baked Gardeniae Fructus, Gardeniae Fructus fried into carbon respectively. One hundred and twenty-four kinds of volatile components were identified by GC-MS. Fifty-three kinds of volatile ingredients consisted in Gardeniae Fructus accounting for 93.85%, 54 kinds in fried Cardeniae Fructus accounting for 92.01%, 32 kinds in stir-baked Cardeniae Fructus accounting for 91.59% and 43 kinds in Gardeniae Fructus fried into carbon accounting for 90.81%. In this paper, analysis of Gardeniae Fructus by GC-MS provides a scientific basis for elucidating the mechanism of different processed products.

摘要

栀子含有挥发成分,然而,不同炮制品中挥发成分的种类和比例有所不同。本实验采用水蒸气蒸馏法分离栀子、炒栀子、焦栀子、栀子炭中的挥发成分,其含量分别为1.2、1.0、0.9、0.7 μL·g-1。通过GC-MS鉴定出124种挥发性成分。栀子中含有53种挥发性成分,占93.85%;炒栀子中含有54种,占92.01%;焦栀子中含有32种,占91.59%;栀子炭中含有43种,占90.81%。本文采用GC-MS对栀子进行分析,为阐明不同炮制品的作用机制提供了科学依据。

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